Titanium oxide particles and method for producing same

The method addresses the challenge of producing titanium oxide particles with fine, uniform sizes and low chlorine content by using a controlled reaction and dechlorination process, ensuring stability and performance in high humidity conditions, suitable for dielectric materials and other applications.

WO2026140228A1PCT designated stage Publication Date: 2026-07-02RESONAC CORP

Patent Information

Authority / Receiving Office
WO · WO
Patent Type
Applications
Current Assignee / Owner
RESONAC CORP
Filing Date
2024-12-27
Publication Date
2026-07-02

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Abstract

This method for producing titanium oxide particles includes: a reaction step for introducing a raw material gas (G1) containing titanium tetrachloride and an inert gas and an oxidizing gas (G2) containing at least one of oxygen gas and water vapor and an inert gas into a reaction tube to generate a reaction gas; a cooling step for introducing a cooling medium and cooling the reaction gas to obtain raw material titanium oxide particles; a first dechlorination step for heating the raw material titanium oxide particles at 300-600°C while bringing water vapor into contact with the raw material titanium oxide particles, the mass ratio (mass of water / mass of raw material titanium oxide particles) of water and raw material titanium oxide particles being 0.01 or more; and a second dechlorination step for heating the raw material titanium oxide particles that have been subjected to the first dechlorination step at 30°C to less than 100°C while bringing water vapor into contact with the raw material titanium oxide particles, the mass ratio (mass of water / mass of raw material titanium oxide particles) of water and raw material titanium oxide particles being 0.01 or more.
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