17-4PH Steel Sintering for Corrosion Resistance

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Solution Overview

Problem

Current selective laser sintering methods lack the capability to produce corrosion-resistant parts from ferrous materials with a wide range of properties, particularly high strength and density.

Innovation Solution

A method involving selective laser sintering of a metal powder mixture with a composition of 15.5-17.5% Cr, 3.5-4.5% Ni, 3.5-4.5% Cu, 0.15-0.45% Cb+Ta, 0.1%-0.3% B, 0-0.5% Mn, 0-0.04% P, 0.07% max C, and balance Fe, using a polymer binder, followed by furnace sintering to achieve a substantially pure martensitic structure and density greater than 7.5 g/cm³.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If selective laser sintering is performed on ferrous materials using conventional methods, then parts can be fabricated with basic mechanical properties, but the parts lack corrosion resistance and high strength characteristics

Engineering Contradiction:
Improvecorrosion resistanceVSAvoidfabrication capability
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent applies parameter changes by precisely controlling the chemical composition parameters of the ferrous powder (specific elements and their ranges) and processing parameters (laser power, scan speed, layer thickness) to transform conventional SLS into a method that produces corrosion-resistant, high-strength parts with density greater than 7.5 g/cm³

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by creating a ferrous powder blend containing multiple elements (Fe, Cr, Ni, Cu, Cb, Ta, B, Mn, P, C) in specific proportions, where each element contributes specific properties that collectively achieve corrosion resistance and high strength in the sintered part

Inventive Principle:
Principle #40Composite materials

2Strength

If conventional SLS processing is used on metal powders, then parts can be formed with standard density, but the parts achieve density less than 7.5 g/cm³ and lack high strength properties

Engineering Contradiction:
Improvetensile strengthVSAvoiddensity control
Core Design Contradiction:
StrengthVSManufacturing precision

Solution Approach 1:

The patent changes processing parameters including laser power, scan speed, hatch spacing, and layer thickness to optimize densification during SLS, achieving density greater than 7.5 g/cm³ and substantially pure martensitic structure that provides high tensile strength

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies local quality by creating a specific microstructure (substantially pure martensitic structure) through controlled cooling and sintering parameters, where the local atomic arrangement and phase distribution are optimized to maximize strength properties

Inventive Principle:
Principle #3Local quality

3Reliability

If ferrous parts are fabricated by conventional methods, then basic mechanical properties can be achieved, but fatigue resistance is insufficient

Engineering Contradiction:
Improvefatigue resistanceVSAvoidprocessing complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent optimizes processing parameters (laser energy density, scan patterns, layer thickness) and compositional parameters (boron content 0.15-0.45%, alloying elements) to control microstructure formation, achieving enhanced fatigue resistance through a dense, uniform martensitic structure without requiring additional post-processing steps

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method effectively produces high-strength, corrosion-resistant ferrous parts with improved density and structural integrity, achieving enhanced mechanical properties such as increased tensile strength and fatigue resistance through optimized boron addition and processing conditions.

Implementation Method 1

Selective laser sintering (SLS) is among the most common commercial available rapid prototyping technologies that fabricates a part by layer-by-layer powder deposition

Methodology Applied
Scientific EffectSelective laser sintering: Selective Laser Sintering

Implementation Method 2

a laser is applied to the powder layer so as to melt the binder material

Methodology Applied
Scientific EffectLaser heating: Laser

Implementation Method 3

the part is transferred to a furnace where the binder is removed and the powder is lightly sintered together

Methodology Applied
Scientific EffectFurnace sintering: Sintering

Implementation Method 4

The brown part is further heated to further sinter the powder together until the final part is formed

Methodology Applied
Scientific EffectThermal processing: Heating

Data Source

PatentEP2150368B1Direct to metal sintering of 17-4PH steel
Publication Date: 2012.05.16 THE BOEING CO
  • EP2150368B1 patent drawingFigure 1
  • EP2150368B1 patent drawingFigure 2
  • EP2150368B1 patent drawingFigure 3

AI summary

A method of sintering a 17-4PH alloy powder and a sintered 17-4PH sintered part are disclosed. The part is formed by selective laser sintering a 17-4PH alloy powder and binder mixture to form a green part that is sintered to form a part having a substantially pure martensitic structure. The metal powder includes boron. The sintered part may be further processed by shot peening to improve crack resistance.