2D Perovskite X-Ray Scintillators With Reduced Re-Absorption Loss

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Solution Overview

Problem

Existing X-ray detectors, particularly those using three-dimensional hybrid metal-halide perovskites, face challenges such as low responsivity at high photon energies, limited carrier-diffusion length, and thermal quenching of X-ray excited luminescence, leading to poor detection efficiency and light yield.

Innovation Solution

The use of two-dimensional hybrid perovskites with large exciton binding energy and Stokes' shift for electromagnetic wave detection, which minimizes thermal quenching and re-absorption losses, resulting in high light yield and short decay times.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If three-dimensional hybrid metal-halide perovskites are used for X-ray detection, then large X-ray absorption cross section is achieved, but thermal quenching of luminescence and low light yield occur

Engineering Contradiction:
ImproveX-ray absorption cross sectionVSAvoidthermal quenching of luminescence
Core Design Contradiction:
Quantity of substanceVSLoss of energy

Solution Approach 1:

The patent changes the structural parameter of the perovskite from three-dimensional to two-dimensional, which fundamentally alters the exciton binding energy and thermal stability characteristics. This parameter change enables the material to maintain high luminescence efficiency under thermal conditions while preserving X-ray absorption capability through the retained heavy atom effect.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs hybrid organic-inorganic perovskite materials with specific compositional design, combining organic cations with metal halide frameworks. This composite structure provides both the heavy atom effect for X-ray absorption and the structural characteristics needed to reduce thermal quenching, achieving a balance between absorption efficiency and luminescence stability.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If film thickness is increased to improve detection probability, then absorption efficiency improves, but carrier diffusion length limitation prevents efficient conversion

Engineering Contradiction:
Improvedetection probabilityVSAvoidcarrier diffusion efficiency
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The patent transitions from three-dimensional perovskite structure to two-dimensional layered structure, which fundamentally changes the carrier transport characteristics. The 2D structure provides enhanced carrier confinement and reduced diffusion length requirements while maintaining thick-film absorption capability, effectively decoupling the trade-off between thickness and carrier collection efficiency.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

3Loss of energy

If two-dimensional perovskites are used to reduce thermal quenching, then light yield improves, but detection efficiency at high energies may be limited

Engineering Contradiction:
Improvethermal quenching resistanceVSAvoiddetection efficiency at high energies
Core Design Contradiction:
Loss of energyVSQuantity of substance

Solution Approach 1:

The patent applies local quality enhancement by incorporating heavy atoms (Pb, I, Br, Cl) specifically within the perovskite structure to provide localized X-ray absorption centers. This localized heavy atom effect maintains high absorption cross-section for high-energy photons while the overall 2D perovskite structure provides thermal stability and high light yield through reduced quenching.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Two-dimensional perovskites exhibit improved detection efficiency and light yield across a broad range of temperatures, with scintillation decay times of less than 8 ns, making them suitable for high-performance X-ray scintillators.

Implementation Method 1

photon-to-current conversion in which a semiconducting material directly converts an incoming radiation into an electrical current

Methodology Applied
Scientific EffectPhotoelectric conversion: Photoelectric Effect

Implementation Method 2

X-ray to UV-visible photon down-conversion in which a scintillator material is coupled to a sensitive photo-detector operating at lower photon energies

Methodology Applied
Scientific EffectX-ray to UV-visible photon down-conversion: Fluorescence

Implementation Method 3

use of two-dimensional hybrid perovskites for electromagnetic wave detection in the form of a scintillator

Methodology Applied
Scientific EffectScintillation: Scintillation

Data Source

PatentEP3491424B1Apparatus for electro-magnetic wave detection
Publication Date: 2025.06.04 THALES SOLUTIONS ASIA
  • EP3491424B1 patent drawingFigure 1a~1e
  • EP3491424B1 patent drawingFigure 2~4
  • EP3491424B1 patent drawingFigure 5a~5c

AI summary

An apparatus for electro-magnetic wave detection is disclosed. The apparatus comprises a two-dimensional perovskite having a polaronic emission Stokes' shifted by at least 50 nm to minimise loss due to re-absorption.