3D Graphene Composite Material Viscosity Control

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Solution Overview

Problem

Composite materials with high carbon loading levels often experience undesirable aggregation, leading to uncontrolled increases in viscosity and unpredictable physical properties, while materials without carbon lack certain desirable properties like controlled brittleness.

Innovation Solution

A composite material is formed by mixing thermoplastic resin with polypropylene-graft-maleic anhydride (PPgMA) and carbon particles, where the carbon particles are self-nucleated 3D graphene with exposed carbon surfaces bonded to PPgMA molecules, maintaining density and rheological profiles within specific tolerances.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If high carbon loading levels are used in composite materials, then desirable properties like controlled brittleness are achieved, but aggregation occurs leading to uncontrolled increases in viscosity and unpredictable physical properties

Engineering Contradiction:
Improvecontrolled brittlenessVSAvoidpredictability of physical properties
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The patent introduces an intermediary substance (such as a dispersant or surface treatment agent) that mediates between the carbon particles and the polymer matrix. This intermediary prevents direct aggregation of carbon particles while maintaining their reinforcing effects, thereby achieving controlled brittleness without uncontrolled viscosity increases or unpredictable physical properties.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent applies local quality by creating localized regions with different carbon particle concentrations or surface treatments within the composite material. This allows certain areas to provide controlled brittleness while other areas maintain better flow characteristics, preventing overall aggregation issues and ensuring predictable bulk properties.

Inventive Principle:
Principle #3Local quality

2Strength

If high carbon loading levels are used in composite materials, then enhanced mechanical properties are achieved, but viscosity increases uncontrollably

Engineering Contradiction:
Improvemechanical propertiesVSAvoidviscosity increase
Core Design Contradiction:
StrengthVSLoss of energy

Solution Approach 1:

An intermediary dispersant or surface treatment agent is introduced to mediate between carbon particles and the polymer matrix, preventing particle aggregation that would otherwise cause uncontrolled viscosity increases while preserving the mechanical property enhancements from high carbon loading.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent employs parameter changes by modifying the surface chemistry or physical state of carbon particles through treatments such as oxidation, coating, or functionalization. These parameter changes alter particle-particle and particle-polymer interactions, enabling high carbon loading without proportional viscosity increases.

Inventive Principle:
Principle #35Parameter changes

3Strength

If carbon particles are added to thermoplastic resin, then flexural modulus is increased, but density deviation from initial resin density occurs

Engineering Contradiction:
Improveflexural modulusVSAvoiddensity control
Core Design Contradiction:
StrengthVSManufacturing precision

Solution Approach 1:

The patent applies parameter changes by carefully controlling the density, size distribution, and surface properties of carbon particles to match or closely approximate the resin matrix. By adjusting these parameters, the composite achieves enhanced flexural modulus while maintaining density within acceptable tolerances of the initial resin density.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses local quality by creating a heterogeneous structure where carbon particles are strategically distributed or clustered in specific regions rather than uniformly dispersed. This allows density enhancement in areas requiring strength while maintaining overall density control within specified tolerances.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composite material achieves a predictable rheological profile and enhanced mechanical properties, including increased flexural modulus and tensile strength, while maintaining density within ±3% of the thermoplastic resin, and exhibits improved processing characteristics.

Implementation Method 1

chemical bonding between carbon atoms provided by at least some of the plurality of carbon particles and their respective adjacent interconnected PPgMA molecules

Methodology Applied
Scientific EffectChemical bonding: Chemical Bonding

Data Source

PatentUS11813774B2Method of producing a composite material including three-dimensional (3D) graphene
Publication Date: 2023.11.14 LYTEN INC
  • US11813774B2 patent drawing
  • US11813774B2 patent drawing
  • US11813774B2 patent drawing

AI summary

A method for continuously producing a composite material is disclosed. In some implementations, the method includes supplying a thermoplastic resin having an initial density, mixing polypropylene-graft-maleic anhydride (PPgMA) formed of a plurality of interconnected PPgMA molecules throughout the thermoplastic resin, distributing a plurality of carbon particles throughout the thermoplastic resin and the plurality of interconnected PPgMA molecules, and forming, by rotational molding, the composite material based on a combination of the thermoplastic resin, the PPgMA, and at least some of the plurality of carbon particles.