3D Structures with Tunable Micro-porosity for High Temperature Stability

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Solution Overview

Problem

Current 3-D printed structures lack high temperature stability and low permittivities over a broad range of electromagnetic frequencies, making them unsuitable for high temperature communication applications.

Innovation Solution

The development of 3-D structures with tunable micro-porosity achieved through the judicious selection of 3-D printing ink and processing conditions, where the air in micro-pores acts as a dielectric modifier, maintaining low permittivities across a broader range of electromagnetic frequencies.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If 3-D structures are made from high temperature polymers, then high temperature stability is improved, but permittivity remains high and does not maintain low values over a broad range of electromagnetic frequencies

Engineering Contradiction:
Improvehigh temperature stabilityVSAvoidpermittivity stability over frequency range
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The patent applies porous materials by incorporating micro-pores into the 3-D printed structure made from high temperature polymers. The air-filled micro-pores act as dielectric modifiers that reduce and stabilize permittivity across a broad range of electromagnetic frequencies while preserving the high temperature stability of the polymer matrix.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The patent creates composite materials by combining high temperature polymers with air-filled micro-pores. This composite structure integrates the thermal stability of the polymer with the dielectric properties of air, achieving both high temperature stability and low, frequency-stable permittivity.

Inventive Principle:
Principle #40Composite materials

2Reliability

If micro-porosity is added to 3-D structures, then permittivity is reduced over a broader frequency range, but manufacturing complexity increases

Engineering Contradiction:
Improvepermittivity stability over frequency rangeVSAvoidmanufacturing process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent applies preliminary action by incorporating porosity-generating agents into the printing ink formulation before the 3-D printing process. This allows micro-pores to form automatically during or after printing through phase separation or solvent evaporation, eliminating the need for subsequent complex post-processing steps to create pores.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent applies parameter changes by modifying the chemical composition of the printing ink to include porosity-generating components. By changing the ink's physical and chemical parameters, the printing process itself generates the desired micro-porous structure, simplifying manufacturing while achieving the target permittivity properties.

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If conventional 3-D printing inks are used, then manufacturing is simple, but micro-porosity cannot be controlled or tuned

Engineering Contradiction:
Improveprinting process simplicityVSAvoidmicro-porosity tunability
Core Design Contradiction:
Ease of manufactureVSAdaptability or versatility

Solution Approach 1:

The patent applies parameter changes by formulating printing inks with adjustable compositional parameters, including porosity-generating agents, solvents, and polymer concentrations. These compositional parameters can be tuned to control the amount, size, and distribution of micro-pores, enabling versatile control over dielectric properties while maintaining the simplicity of the printing process.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent develops composite printing inks that combine polymers, solvents, and porosity-generating agents in adjustable ratios. By varying the composition parameters of this composite ink system, manufacturers can tune the resulting micro-porosity to achieve specific permittivity values and frequency responses without complicating the printing process.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The resulting 3-D structures exhibit improved high temperature stability and low permittivities, enhancing communication performance in high temperature environments, particularly in communication devices like array antennas.

Implementation Method 1

the air in the 3-D structure's micro-pores acts as a dielectric modifier. Thus, low permittivities over a broader range of electromagnetic frequencies can be obtained from the 3-D structure

Methodology Applied
Scientific EffectDielectric: Dielectric

Data Source

PatentUS11787109B13-d structures having high temperature stability and improved microporosity
Publication Date: 2023.10.17 THE GOVERNMENT OF THE UNITED STATES AS REPRESENTED BY THE SECRETARY OF THE AIR FORCE
  • US11787109B1 patent drawing
  • US11787109B1 patent drawing
  • US11787109B1 patent drawing

AI summary

The present invention relates to 3-D structures having high temperature stability and improved micro-porosity as well as processes of making and using same. The disclosed 3-D are advantageous because they have low densities and low permittivities. When compared to previous 3-D structures, the present structures maintain their low permittivities over a broader range of electromagnetic frequencies. Thus, when used in communication devices such as array antennas, can provided higher communication performance in high temperature environments.