AAV Formulation Stability via Buffering and Surfactant Mediation

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Solution Overview

Problem

Current AAV formulations for human administration face challenges in maintaining long-term stability, preventing adsorption to surfaces, and minimizing potency loss during manufacturing and storage, despite efforts to design safe and effective formulations.

Innovation Solution

The development of pharmaceutical compositions comprising AAV, buffering agents, pharmaceutically acceptable salts, non-ionic surfactants, and sugars or sugar alcohols, which are formulated to prevent adsorption and maintain potency, including specific concentrations of L-histidine, sodium chloride, polysorbate 80, and sucrose or trehalose, and can be either liquid or lyophilized for enhanced stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If AAV formulations are designed for long-term storage, then stability is improved, but adsorption to container surfaces and potency loss occur

Engineering Contradiction:
ImproveAAV stabilityVSAvoidAAV potency loss
Core Design Contradiction:
Stability of the object's compositionVSLoss of substance

Solution Approach 1:

The patent introduces a specific formulation composition including buffering agents (pH 6.0-8.0), salts (50-150 mM), non-ionic surfactants (0.001-0.01% w/v), and sugars or sugar alcohols (1-10% w/v) as intermediary substances that mediate between the AAV and the storage environment, preventing direct harmful interactions with container surfaces while maintaining viral stability during long-term storage

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent optimizes specific formulation parameters including pH (6.0-8.0), salt concentration (50-150 mM), surfactant concentration (0.001-0.01% w/v), and sugar/sugar alcohol content (1-10% w/v) to achieve the optimal balance between stability and prevention of potency loss, demonstrating that precise parameter control resolves the contradiction

Inventive Principle:
Principle #35Parameter changes

2Stability of the object's composition

If AAV formulations use high salt concentrations, then stability is improved, but adsorption to surfaces increases

Engineering Contradiction:
ImproveAAV stabilityVSAvoidAdsorption to surfaces
Core Design Contradiction:
Stability of the object's compositionVSObject-affected harmful factors

Solution Approach 1:

The patent identifies and optimizes the salt concentration parameter within a specific range (50-150 mM) to achieve optimal stability while minimizing surface adsorption, demonstrating that precise parameter control resolves the contradiction between stability and adsorption

Inventive Principle:
Principle #35Parameter changes

3Duration of action of stationary object

If AAV formulations are stored for extended periods, then long-term stability is achieved, but visible particle formation occurs

Engineering Contradiction:
ImproveStorage durationVSAvoidVisible particle formation
Core Design Contradiction:
Duration of action of stationary objectVSObject-generated harmful factors

Solution Approach 1:

The patent introduces sugars or sugar alcohols (1-10% w/v) and non-ionic surfactants as intermediary protective agents that prevent direct aggregation and visible particle formation during extended storage periods, allowing long-term stability without degradation

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The formulation includes protective agents (sugars, sugar alcohols, surfactants) that provide beforehand cushioning against degradation mechanisms, preventing visible particle formation before it can occur during extended storage

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

These formulations effectively prevent visible particle formation, reduce degradation, and maintain significant AAV activity over extended periods, ensuring stability and potency during storage and administration.

Implementation Method 1

about 5 mM to about 25 mM of a buffering agent

Methodology Applied
Scientific EffectBuffering:

Implementation Method 2

about 0.001% (w/v) to about 0.01% (w/v) of a non-ionic surfactant

Methodology Applied
Scientific EffectSurfactant: Surfactant

Implementation Method 3

about 1% (w/v) to about 10% (w/v) of a sugar or sugar alcohol

Methodology Applied
Scientific EffectSolvation: Solvation

Data Source

PatentUS12257277B2Adeno-associated virus formulations
Publication Date: 2025.03.25 TAKEDA PHARMA CO LTD

AI summary

Adeno-associated liquid and lyophilized pharmaceutical compositions are provided herein. In exemplary aspects, the pharmaceutical compositions comprise about 5 mM to about 25 mM L-histidine, about 0 mM to about 150 mM sodium chloride, about 0.001% (w/v) to about 0.01% (w/v) polysorbate 80 (PS80), and about 1% to about 10% (w/v) sucrose, trehalose, or combination thereof to AAV. In exemplary aspects, the pharmaceutical compositions further comprise glycine or mannitol. Methods of preparing a pharmaceutical composition comprising AAV, methods of treating a bleeding disorder in a subject, and methods of storing AAV compositions are also provided.