Acacia crassicarpa Dissolving Pulp Production via Pre-hydrolysis Kraft Process

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Solution Overview

Problem

The production of dissolving pulp from alternative hardwood species has been limited due to difficulties in reducing silica content and managing lipophilic extractives, which affect the pulping process and quality of the pulp, making it challenging to meet stringent industrial requirements.

Innovation Solution

The use of Acacia crassicarpa as a raw material for producing dissolving pulp, which has a low lipophilic content, allowing for the production of pulp with high alpha cellulose content and improved operability, through a pre-hydrolysis Kraft process that includes hydrolysis and alkaline treatment to degrade hemicelluloses and lignin, resulting in a pulp suitable for viscose fiber production.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If alternative hardwood species are used to produce dissolving pulp, then material availability and cost are improved, but the lipophilic extractives content increases making it difficult to meet industrial requirements

Engineering Contradiction:
Improvematerial availabilityVSAvoidlipophilic extractives content
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The patent applies extraction by selecting Acacia crassicarpa wood chips as the raw material, which naturally contains low levels of lipophilic extractives (0.03-0.20 wt%). This extraction principle works at the material selection stage rather than requiring post-processing removal, thereby achieving both availability and quality requirements simultaneously

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent changes the key parameter of lipophilic extractives content by selecting a specific wood species (Acacia crassicarpa) with inherently low extractive content (0.03-0.20 wt%). This parameter change at the raw material level enables the pulp to meet stringent industrial specifications without requiring additional extraction processes

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If alternative hardwood species are used to produce dissolving pulp, then material availability is improved, but the silica content increases making it difficult to meet industrial requirements

Engineering Contradiction:
Improvematerial availabilityVSAvoidsilica content
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The patent applies extraction by selecting Acacia crassicarpa wood chips as the raw material, which naturally contains low levels of silica (0.01-0.05 wt%). This extraction principle works at the material selection stage rather than requiring post-processing removal, thereby achieving both availability and quality requirements simultaneously

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent changes the key parameter of silica content by selecting a specific wood species (Acacia crassicarpa) with inherently low silica content (0.01-0.05 wt%). This parameter change at the raw material level enables the pulp to meet stringent industrial specifications without requiring additional removal processes

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If conventional hardwood species are used to produce dissolving pulp, then the pulping process is well-established, but the lipophilic extractives content is high requiring extensive treatment

Engineering Contradiction:
Improvepulping process establishmentVSAvoidlipophilic extractives content
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The patent changes the key parameter of lipophilic extractives content by selecting Acacia crassicarpa wood chips with inherently low extractive content (0.03-0.20 wt%). This parameter change at the raw material level eliminates the need for extensive extractive removal treatments while maintaining ease of manufacture through conventional pulping processes

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies extraction by selecting Acacia crassicarpa wood chips as the raw material, which naturally contains low levels of lipophilic extractives. This extraction principle works at the material selection stage rather than requiring post-processing removal, thereby achieving both availability and quality requirements simultaneously

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Acacia crassicarpa-based dissolving pulp meets commercial specifications with high alpha cellulose content and low lipophilic extractives, enhancing the yield and quality of the pulp, and facilitating the production of strong, uniform viscose fibers.

Implementation Method 1

hydrolysing a composition comprising cellulosic or a lignocellulosic material consisting of Acacia crassicarpa to thereby form a treated cellulosic or lignocellulosic composition

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 2

heating the treated composition under conditions to produce said dissolving pulp

Methodology Applied
Scientific EffectOxidation: Oxidation

Data Source

PatentEP3093389B1Dissolving pulp
Publication Date: 2019.11.13 PT ASIA PACIFIC RAYON
  • EP3093389B1 patent drawingFigure 1~2
  • EP3093389B1 patent drawingFigure 3~4
  • EP3093389B1 patent drawingFigure 5

AI summary

There is provided a dissolving pulp, a cellulosic composition, a composition, regenerated cellulose fibre and a textile comprising Acacia crassicarpa. There is provided the use of the compositions for preparing a dissolving pulp. There is provided a method of preparing dissolving pulp, comprising: (a) hydrolysing a composition comprising cellulosic or a lignocellulosic material of Acacia crassicarpa to thereby form a treated cellulosic or lignocellulosic composition; (b) heating the treated composition under conditions to produce said dissolving pulp; and a method of producing regenerated cellulose fibres, comprising: (a) base treatment of a dissolving pulp of Acacia crassicarpa to produce cellulose xanthate; (b) neutralizing said cellulose xanthate to produce said regenerated cellulose fibres.