Acoustic Agglomeration Detection in Gas Phase Reactors

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Solution Overview

Problem

The formation of particle agglomerations in gas phase reactors during catalytic polyolefine production leads to disturbances in hydrodynamic flow and temperature distribution, resulting in polymer particles with varying properties and potential reactor blockages, necessitating an efficient detection and control system to prevent reactor shutdowns.

Innovation Solution

A control system that detects changes in operational parameters of the agitation device, such as vibration and power consumption, to generate control signals that influence the formation or removal of agglomerations, using manipulated variables like flowrate adjustments and antistatic agents, and triggers alarms for operator intervention.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If particle agglomerations are detected using visual detection through windows, then operator observation is enabled, but automatic operation is not achieved and the method is not suitable for automated processes

Engineering Contradiction:
Improveautomatic operationVSAvoiddetection system complexity
Core Design Contradiction:
Ease of operationVSDevice complexity

Solution Approach 1:

The patent replaces mechanical/visual detection methods with acoustic detection using microphones and signal processing systems. The acoustic detection system captures sound signals from the fluidized bed, processes them through spectral analysis, and automatically detects agglomerations without requiring visual observation through windows or manual intervention, thereby enabling automated operation.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Measurement precision

If complex devices are used to measure differential pressure differences for agglomeration detection, then detection capability is improved, but the device complexity increases significantly

Engineering Contradiction:
Improveagglomeration detection capabilityVSAvoiddetection device complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent introduces acoustic signals as an intermediary parameter to detect agglomerations. Instead of directly measuring complex differential pressure differences, the system uses microphones to capture sound waves generated by particle motion, which serve as an indirect but simpler indicator of agglomeration events, reducing device complexity while maintaining detection precision.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent replaces complex mechanical pressure measurement devices with acoustic sensing systems. The microphone-based detection system converts mechanical particle movements into acoustic signals that can be processed electronically, simplifying the overall detection apparatus while maintaining the ability to detect agglomerations.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Measurement precision

If detection rods with magnetic flux measurement are inserted into the reactor, then agglomeration detection is enabled, but operational and structural complexity increases

Engineering Contradiction:
Improveagglomeration detectionVSAvoidstructural complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent extracts the detection function from intrusive physical devices and places it outside the reactor vessel. Acoustic sensors are positioned externally to capture sound waves transmitted through the reactor wall, eliminating the need to insert detection rods into the reactor and thereby reducing structural complexity while maintaining detection capability.

Inventive Principle:
Principle #2Taking out (Extraction)

4Measurement precision

If particle agglomerations form and grow in size, then detection becomes more evident, but reactor blockages occur and productivity decreases

Engineering Contradiction:
Improveagglomeration detectionVSAvoidreactor operation continuity
Core Design Contradiction:
Measurement precisionVSProductivity

Solution Approach 1:

The patent implements preliminary detection of agglomerations at early stages using acoustic signal analysis. By detecting changes in sound spectra before agglomerations grow to block reactor components, the system enables early intervention through automated responses such as adjusting operating parameters or triggering alarms, thereby preventing productivity loss from reactor shutdowns.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent establishes a feedback loop where acoustic detection signals continuously monitor the fluidized bed condition and automatically trigger control responses. When agglomerations are detected through spectral analysis, the system provides feedback to control mechanisms that can adjust operational parameters or activate mitigation strategies, maintaining continuous reactor operation and preventing blockages.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system effectively detects and mitigates particle agglomerations, preventing reactor blockages and maintaining optimal process conditions by automatically adjusting operational parameters and alerting operators to potential issues, thereby ensuring continuous operation.

Implementation Method 1

The operational parameter is selected from the vibration, torque and / or the power consumption of the agitation device

Methodology Applied
Scientific EffectVibration: Vibration

Data Source

PatentEP2397221B1Control system for a gas phase reactor, a gas phase reactor for catalytic production of polyolefines, a method for catalytic productions of polyolefines and a use of the control system
Publication Date: 2017.04.12 BOREALIS AG
  • EP2397221B1 patent drawing
  • EP2397221B1 patent drawing
  • EP2397221B1 patent drawing

AI summary

Control system for a gas phase reactor, a gas phase reactor for catalytic production of polyolefines, a method for catalytic productions of polyolefines and a use of the control system. The invention relates to a control system for a fluidized bed gas phase reactor (100) for the catalytic production of polyolefines having at least one agitation device (1) in a fluidized bed (10) in a gas phase reactor (100), characterized by a detection device (20) for detecting a change (30) in at least one operational parameter of the agitation device (1), in particular the vibration, torque and / or the power consumption of the agitation device (1), the detection device (20) comprising means for the generation of at least one control signal (40) in dependence on the change (30), the control signal (40) acting on a manipulated variable of the gas phase reactor (100), the fluidized bed (10) and / or the agitation device (1) to influence the formation of particle agglomerations in the gas phase reactor (100) and / or the removal of particle agglomerations from the gas phase reactor (100). The invention also relates to a gas phase reactor (100), a method and a use of the control system.