Acrylic Polymer Particles Electrostatic Buildup Inhibition

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Solution Overview

Problem

Particles of acrylic polymer obtained by existing methods suffer from electrostatic buildup, leading to low fluidity and solubility issues, particularly when dissolved in organic solvents like toluene, which affects their handling and application in coating and ink compositions.

Innovation Solution

The development of acrylic polymer particles with a specific composition containing units derived from methyl methacrylate and (meth)acrylic acid alkyl esters, along with controlled sodium element amounts and particle diameters, combined with a washing process using sodium-containing solutions, to inhibit electrostatic buildup and enhance fluidity and solubility.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If particles of acrylic polymer are produced by conventional suspension polymerization method, then production cost is reduced, but electrostatic buildup occurs leading to poor fluidity

Engineering Contradiction:
Improveproduction costVSAvoidfluidity
Core Design Contradiction:
Ease of manufactureVSEase of operation

Solution Approach 1:

The patent changes the chemical composition parameters of the acrylic polymer particles by incorporating specific functional groups (carboxyl groups at 0.1-10 mmol/g and hydroxyl groups at 0.1-10 mmol/g) to alter the surface properties. This modifies the electrostatic characteristics without changing the fundamental production method, thereby maintaining low production cost while improving fluidity through suppressed electrostatic buildup.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces electrolytes as an intermediary substance during the washing process. The electrolyte solution (containing salts like NaCl, Na2SO4, or NaHCO3 at 0.1-10 g/L) acts as a mediator to neutralize electrostatic charges on the particle surfaces during washing, preventing electrostatic buildup without requiring expensive anti-static additives or equipment modifications.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Device complexity

If conventional drying methods are used after suspension polymerization, then production process is simplified, but electrostatic buildup increases

Engineering Contradiction:
Improveprocess complexityVSAvoidelectrostatic buildup
Core Design Contradiction:
Device complexityVSEase of operation

Solution Approach 1:

The patent applies preliminary action by incorporating electrolyte treatment during the washing step before drying. This preliminary introduction of electrolytes prevents electrostatic buildup from occurring in the first place during subsequent drying operations, eliminating the need for complex post-drying anti-static treatments or specialized drying equipment.

Inventive Principle:
Principle #10Preliminary action

3Reliability

If particles are washed with pure water, then purity is maintained, but electrostatic buildup inhibition is insufficient

Engineering Contradiction:
ImprovepurityVSAvoidelectrostatic buildup inhibition
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The patent changes the washing parameter from pure water to an electrolyte-containing aqueous solution. This modification introduces ions (Na+, Cl-, SO4 2-, HCO3 -) at controlled concentrations (0.1-10 g/L) that suppress electrostatic charges on particle surfaces while maintaining the washing function and overall purity of the polymer particles.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The approach results in particles with excellent fluidity and solubility, reducing the risk of clogging and improving handling, while maintaining purity and enhancing the performance of coating and ink compositions.

Implementation Method 1

the particles having electrostatic buildup inhibition rate of 90 to 99.9%

Methodology Applied
Scientific EffectElectrostatic buildup inhibition: Electrostatics

Data Source

PatentUS11472893B2Acrylic polymer particles, production process therefor, ink composition, and coating composition
Publication Date: 2022.10.18 MITSUBISHI CHEM CORP

AI summary

Particles of an acrylic polymer comprising a constituent unit (A) derived from methyl methacrylate and a constituent unit (B) derived from a (meth)acrylic acid alkyl ester in which the alkyl group has 2 to 8 carbon atoms, wherein the particles having electrostatic buildup inhibition rate of 90 to 99.9° as obtained by a specific method.