Actinically Curable Adhesive Composition for Flexible Packaging

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Solution Overview

Problem

Current adhesives for flexible packaging laminates face limitations such as the presence of volatile organic compounds (VOCs), flammability, residual solvents, lengthy curing times, and issues with two-component systems, which affect bond strength, chemical resistance, and safety for food and pharmaceutical packaging.

Innovation Solution

An actinically curable adhesive composition comprising an inert urethane polymer and an ethylenically unsaturated component, which is dispersed and cured using actinic radiation, providing a one-component, solventless system with fast curing and strong bond formation without VOCs or toxic byproducts.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If organic solvent base adhesives are used, then bond strength is achieved, but volatile organic compounds (VOCs) are present and flammability issues arise

Engineering Contradiction:
Improvebond strengthVSAvoidVOCs and flammability
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The patent changes the chemical composition parameters by using isocyanate-terminated polyurethane prepolymers with specific molecular weights (2,000-10,000) and controlled NCO content (1-5%), eliminating organic solvents while maintaining adhesive performance through precise molecular parameter control

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates an inert chemical environment by using water as the continuous phase instead of organic solvents, and by controlling the reaction environment to prevent unwanted side reactions, thereby eliminating VOC emissions and flammability hazards

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

2Object-affected harmful factors

If water based adhesives are used, then VOCs are eliminated, but drying equipment is required and drying time is needed

Engineering Contradiction:
ImproveVOC eliminationVSAvoiddrying time
Core Design Contradiction:
Object-affected harmful factorsVSLoss of time

Solution Approach 1:

The patent extracts and eliminates the drying step entirely by using a one-component system that cures through moisture reaction or heat activation, removing the time-consuming evaporation process required by traditional water-based adhesives

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent replaces the mechanical drying process (evaporation requiring drying equipment) with a chemical curing mechanism that occurs in-situ, substituting a time-intensive physical process with a faster chemical transformation

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Strength

If two component systems are used, then bond strength is improved, but mixing consistency and pot life management become difficult

Engineering Contradiction:
Improvebond strengthVSAvoidmixing consistency and pot life
Core Design Contradiction:
StrengthVSEase of operation

Solution Approach 1:

The patent merges the adhesive and curing agent into a single pre-formulated one-component system containing isocyanate-terminated polyurethane prepolymer, eliminating the need for separate mixing of multiple components while maintaining the crosslinked network structure for strong bonds

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent performs the curing agent preparation in advance by synthesizing isocyanate-terminated prepolymers with controlled molecular weights and NCO content before application, so that no on-site mixing is required and the adhesive is ready for immediate use with extended operational stability

Inventive Principle:
Principle #10Preliminary action

4Strength

If two component systems are used, then adhesive properties are improved, but curing time becomes lengthy (2 to 5 days)

Engineering Contradiction:
Improveadhesive propertiesVSAvoidcuring time
Core Design Contradiction:
StrengthVSLoss of time

Solution Approach 1:

The patent changes the curing kinetics by using pre-formed isocyanate-terminated prepolymers with specific molecular weights and reactivity, enabling rapid crosslinking upon application that reduces curing time from days to hours or minutes while maintaining network integrity

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent performs the complex polymer synthesis and functional group preparation in advance during manufacturing, creating prepolymers with built-in reactivity that eliminates the lengthy mixing and reaction time required when combining separate components on-site

Inventive Principle:
Principle #10Preliminary action

5Loss of time

If UV curable adhesives are used, then fast curing is achieved, but transparent substrates are required

Engineering Contradiction:
Improvecuring speedVSAvoidsubstrate transparency requirement
Core Design Contradiction:
Loss of timeVSAdaptability or versatility

Solution Approach 1:

The patent creates a universal adhesive system that can cure on both transparent and opaque substrates by using moisture reaction or heat activation mechanisms that do not depend on light penetration, making the adhesive applicable to a broader range of packaging materials including metals, pigmented plastics, and printed surfaces

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The adhesive composition achieves rapid curing, strong lamination bonds, and improved safety for food and pharmaceutical packaging by eliminating VOCs and toxic byproducts, with the ability to bond opaque substrates and offering long shelf-life and low shrinkage.

Implementation Method 1

Radiation-curable laminating adhesives for flexible packaging should provide sufficient bond strength and chemical resistance

Methodology Applied
Scientific EffectPhotopolymerization: Photopolymerisation

Implementation Method 2

EB radiation has the advantage of being able to penetrate opaque or printed packaging materials in order to cure the adhesive

Methodology Applied
Scientific EffectElectron beam curing: Electron Beam

Data Source

PatentEP3700975B1Actinically curable adhesive composition with improved properties
Publication Date: 2023.12.06 SUN CHEMICAL CORP

AI summary

Described herein is an actinically curable adhesive composition, suitable for sealing flexible packaging, that includes an inert urethane polymer and an ethylenically unsaturated monomer component selected from at least one monofunctional ethylenically unsaturated monomer, at least one multifunctional ethylenically unsaturated monomer, and a combination thereof, wherein the ethylenically unsaturated monomer component disperses the inert urethane polymer. The compositions are suitable for forming flexible packaging materials for foods and other materials, particularly sensitive materials. Also described are flexible packaging materials and a method for preparing an actinically curable adhesive composition.