Adiabatic Expansion Piston for Liquid Component Separation

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Solution Overview

Problem

Traditional separation processes, such as distillation and crystallization, are often expensive, energy-intensive, and complex, failing to completely separate solid components from other phases due to incomplete separation, leaving residual contaminants.

Innovation Solution

A vessel with a piston is used to separate components by expanding the inner chamber volume, causing the first component to vaporize and the second component to freeze, with the vapor stream being expelled and the solid product stream extruded through a solids outlet, effectively converting a liquid-liquid separation into a gas-solid separation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If traditional separation processes like distillation and absorption are used, then fluid purity is increased, but energy consumption increases and complete separation is not achieved

Engineering Contradiction:
Improveseparation completenessVSAvoidenergy consumption
Core Design Contradiction:
Manufacturing precisionVSUse of energy by moving object

Solution Approach 1:

The invention utilizes rapid phase transitions (freezing and vaporization) achieved through adiabatic expansion to separate components. When the liquid mixture undergoes sudden expansion, one component freezes into solid particles while another vaporizes, creating a gas-solid mixture that can be completely separated through cyclonic separation, achieving complete separation without high energy consumption

Inventive Principle:
Principle #36Phase transitions

Solution Approach 2:

The invention changes the thermodynamic parameters (pressure and temperature) of the liquid mixture through adiabatic expansion. By rapidly decreasing pressure and temperature, the system induces phase transitions that enable complete separation of components, overcoming the limitation of traditional processes that cannot achieve complete separation

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If traditional separation processes are used, then some purification is achieved, but residual contaminants remain in all phases

Engineering Contradiction:
ImprovepurityVSAvoidcontaminant elimination
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

By inducing simultaneous freezing and vaporization through adiabatic expansion, the invention creates distinct solid and gas phases that can be completely separated. The solid component freezes into particles while the other component vaporizes, allowing for complete separation via cyclonic separation, eliminating residual contaminants that persist in traditional processes

Inventive Principle:
Principle #36Phase transitions

Solution Approach 2:

The invention extracts one component from the liquid mixture by freezing it into solid particles through adiabatic expansion. These solid particles are then completely separated from the vapor phase using cyclonic separation, effectively removing one component entirely from the mixture and achieving complete purification

Inventive Principle:
Principle #2Taking out (Extraction)

3Manufacturing precision

If complex separation equipment is used, then separation effectiveness is improved, but device complexity increases

Engineering Contradiction:
Improveseparation effectivenessVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The invention uses natural phase transitions induced by adiabatic expansion to perform separation, replacing complex multi-stage separation equipment. The sudden pressure drop causes one component to freeze and another to vaporize, and a simple cyclone separator accomplishes what would otherwise require complex distillation or filtration systems

Inventive Principle:
Principle #36Phase transitions

Solution Approach 2:

The invention replaces complex mechanical separation systems with a thermodynamic approach using adiabatic expansion and phase transitions. Instead of using multiple mechanical separation stages, the system uses pressure-induced phase changes followed by simple cyclonic separation, dramatically reducing device complexity while maintaining high separation effectiveness

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enables a simple and thermodynamically efficient separation of liquid components, eliminating residual contaminants and reducing energy costs by utilizing the heat of vaporization for solid formation and expelling the vapor stream, while extruding the solid product.

Implementation Method 1

The piston is retracted to a second position such that a volume of the inner chamber increases to a second volume, causing the first component and a first portion of the second component to flash to form a vapor stream while a second portion of the second component freezes

Methodology Applied
Scientific EffectAdiabatic expansion: Adiabatic Cooling

Implementation Method 2

causing the first component and a first portion of the second component to flash to form a vapor stream while a second portion of the second component freezes to form a solid product stream

Methodology Applied
Scientific EffectPhase change: Phase Change

Implementation Method 3

utilizing the heat of vaporization for solid formation

Methodology Applied
Scientific EffectHeat of vaporization: Latent Heat

Implementation Method 4

The piston is advanced to a third position that results in a third volume, smaller than the first volume, such that the vapor stream is expelled

Methodology Applied
Scientific EffectPressure increase: Pressure Increase

Implementation Method 5

The piston is fully closed such that the solid product stream is pressed into and extruded through the solids outlet

Methodology Applied
Scientific EffectMechanical force: Mechanical Force

Data Source

PatentUS11325087B2Devices and methods for separating components
Publication Date: 2022.05.10 U S BANK TRUST CO NAT ASSOC
  • US11325087B2 patent drawing
  • US11325087B2 patent drawing
  • US11325087B2 patent drawing

AI summary

A method, system, and device for separating components is described. A vessel is provided. A first volume of a process liquid, containing a first component and a second component, is passed into an inner chamber. The piston retracts to a first position. The fluid inlet is closed. The piston is retracted to a second position, causing the first component and a first portion of the second component to flash to form a vapor stream while a second portion of the second component freezes to form a solid product stream. The fluid outlet is then opened. The piston is advanced to a third position that results in a third volume, smaller than the first volume, such that the vapor stream is expelled. The fluid outlet is closed. The piston is fully closed such that the solid product stream is pressed into and extruded through the solids outlet.