Aerosol Substrate Viscosity Control via Pre-dissolved Binder

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Solution Overview

Problem

Aerosol-forming substrates often experience agglomeration and high viscosity issues due to low solubility of components, leading to difficult handling and excessive foaming during production, which complicates the production and storage of these substrates.

Innovation Solution

A method involving the formation of a first slurry with hydroxypropylmethyl cellulose, water, and an aerosol-former, with a viscosity of 0.9 Pa·s to 5 Pa·s, allowing for easy mixing and processing without the need for dough mixer equipment, and subsequent combination with a cellulose-based strengthening agent and binder to create a final slurry that can be easily dried, reducing foam formation and agglomeration.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If components are mixed to form aerosol-forming substrate, then the substrate is formed with necessary components, but agglomeration and high viscosity occur making the solution difficult to handle

Engineering Contradiction:
Improveease of handlingVSAvoidviscosity
Core Design Contradiction:
Ease of manufactureVSDevice complexity

Solution Approach 1:

The binder is pre-dissolved in water to create a binder solution before mixing with other components. This preliminary action ensures the binder is fully dissolved and distributed, preventing localized high-viscosity regions and agglomeration during subsequent mixing operations

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent specifies controlling the viscosity of the first slurry (hydroxypropylmethyl cellulose, water, and aerosol-former mixture) to be between 0.9 Pa·s and 5 Pa·s. By controlling this parameter, the mixture remains handleable while achieving adequate film-forming properties

Inventive Principle:
Principle #35Parameter changes

2Ease of manufacture

If components are mixed to form aerosol-forming substrate, then the substrate is formed with necessary components, but excessive foaming occurs complicating handling

Engineering Contradiction:
Improveease of handlingVSAvoidfoaming
Core Design Contradiction:
Ease of manufactureVSObject-generated harmful factors

Solution Approach 1:

The binder is pre-dissolved in water before mixing with other components. This preliminary dissolution prevents air entrapment and foam formation during mixing, as the binder solution provides a uniform base that reduces气穴 formation

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The controlled viscosity range (0.9-5 Pa·s) of the first slurry affects foam stability and formation. This viscosity range allows adequate mixing while minimizing foam generation and facilitating foam collapse if it does form

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If hydroxypropylmethyl cellulose and binder are directly mixed, then all components are combined, but a dough-like mixture with very high viscosity is formed that is difficult to handle and pump

Engineering Contradiction:
Improveease of handlingVSAvoidviscosity
Core Design Contradiction:
Ease of manufactureVSDevice complexity

Solution Approach 1:

The mixing process is segmented into distinct stages: first preparing a hydroxypropylmethyl cellulose slurry with controlled viscosity, then separately preparing a binder solution, and finally combining them. This segmentation prevents the formation of a dough-like mixture by ensuring proper dispersion at each stage

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Water serves as an intermediary medium that facilitates the separate dissolution of hydroxypropylmethyl cellulose and binder before their combination. The water-based slurries act as intermediaries that prevent direct interaction between the two polymers that would otherwise create high-viscosity dough-like mixtures

Inventive Principle:
Principle #24Intermediary (Mediator)

4Productivity

If slurry is dried to produce aerosol-forming substrate, then the substrate is obtained, but the drying process takes time

Engineering Contradiction:
Improvedrying speedVSAvoiddrying time
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The controlled viscosity and composition of the final slurry (achieved through proper mixing ratios and the use of hydroxypropylmethyl cellulose) optimize drying characteristics. The slurry formulation allows for faster evaporation of the aerosol-former and water, reducing drying time while maintaining substrate quality

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method results in an aerosol-forming substrate with improved handling and drying properties, allowing for stable storage and efficient production by maintaining sufficient viscosity for easy processing and reducing the formation of agglomerates and foam, facilitating the production of aerosol-forming substrates with enhanced cohesion and gel properties.

Implementation Method 1

the first slurry having a viscosity of between 0.9 Pa·s and 5 Pa·s, preferably between 0.9 Pa·s and 4 Pa·s

Methodology Applied
Scientific EffectViscosity:

Implementation Method 2

The final slurry is dried in order to obtain the aerosol-forming substrate

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS20240298695A1Method for producing an aerosol-forming substrate and aerosol-forming substrate
Publication Date: 2024.09.12 PHILIP MORRIS PRODUCTS SA
  • US20240298695A1 patent drawing
  • US20240298695A1 patent drawing

AI summary

The invention relates to a method for producing an aerosol-forming substrate comprising: providing a cellulose based strengthening agent, providing a binder, mixing of hydroxypropylmethyl cellulose, water and an aerosol-former to form a first slurry, the first slurry having a viscosity of between 0.9 Pa s and 5 Pa s, and combining the cellulose based strengthening agent, the binder and the first slurry in order to obtain a final slurry, and drying the final slurry to obtain the aerosol-forming substrate. This method provides a first slurry having reduced viscosity and less water content.