Al-Coated Ni-Mn Cathode Particles for High-Voltage Cycle Stability

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Solution Overview

Problem

The demand for high-capacity, high-energy-density rechargeable lithium batteries is increasing, but the supply of cobalt, a rare and expensive metal, is limited, and existing cobalt-free positive electrode active materials face challenges in maintaining structural stability, resistance, and cycle-life characteristics under high-voltage and high-temperature conditions.

Innovation Solution

A positive electrode active material comprising a layered lithium nickel-manganese-based composite oxide with an aluminium coating layer on the surface of core particles, where the material is formed by agglomerating primary particles into secondary particles, and smaller single particles with a thinner aluminium coating, enhancing structural stability and reducing side reactions with electrolytes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If cobalt-free positive electrode active materials are used to reduce cost and supply dependency, then production cost decreases and supply security improves, but structural stability and performance under high-voltage and high-temperature conditions deteriorate

Engineering Contradiction:
Improveproduction costVSAvoidstructural stability
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

An aluminium coating layer is introduced as an intermediary substance between the cobalt-free positive electrode active material and the electrolyte. This coating layer mediates the interaction by providing structural support and protecting the underlying active material from degradation under high-voltage and high-temperature conditions, thereby improving reliability without compromising the cost benefits of cobalt-free composition

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention creates a composite structure consisting of cobalt-free positive electrode active material combined with an aluminium coating layer. This composite material approach allows the system to benefit from the cost advantages of cobalt-free materials while the aluminium coating provides the necessary structural stability and performance characteristics under extreme operating conditions

Inventive Principle:
Principle #40Composite materials

2Reliability

If aluminium coating layer is applied to improve structural stability and reduce side reactions, then reliability and cycle-life characteristics improve, but manufacturing complexity increases

Engineering Contradiction:
Improvecycle-life characteristicsVSAvoidmanufacturing complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The invention optimizes specific parameters of the aluminium coating layer including thickness (5-50 nm), aluminium content (0.1-5 at%), and crystal structure to achieve the desired balance between reliability improvement and manufacturing complexity. By controlling these parameters within specific ranges, the coating provides effective protection while maintaining manufacturability

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If high energy density is achieved through optimized composition and structure, then capacity and energy density improve, but resistance to side reactions with electrolytes under high-voltage conditions worsens

Engineering Contradiction:
Improveenergy densityVSAvoidside reactions with electrolytes
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The aluminium coating layer serves as a protective intermediary that prevents direct contact between the high-energy-density active material and the electrolyte. This intermediary layer blocks harmful side reactions while allowing the underlying material to maintain its high capacity and energy density characteristics

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The aluminium coating layer acts as a sacrificial protective layer that can be consumed or degraded preferentially to protect the valuable high-energy-density active material. This approach allows the system to achieve high energy density while the coating absorbs the damage from side reactions with electrolytes

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves high energy density, improved capacity, and extended cycle-life characteristics under high-voltage and high-temperature conditions while minimizing production costs by using a cobalt-free composition and optimizing the aluminium coating layer.

Implementation Method 1

an aluminium coating layer on the surface of the core particle

Methodology Applied
Scientific EffectCoatings: Coatings

Implementation Method 2

layered lithium nickel-manganese-based composite oxide... maximize or increase capacity (e.g., electrical capacity)

Methodology Applied
Scientific EffectIon insertion/extraction: Absorption (physical)

Data Source

PatentEP4607616A1Positive electrode active materials, positive electrodes, and rechargeable lithium batteries
Publication Date: 2025.08.27 SAMSUNG SDI CO LTD
  • EP4607616A1 patent drawingFigure 1
  • EP4607616A1 patent drawingFigure 2
  • EP4607616A1 patent drawingFigure 3

AI summary

A positive electrode active material, a positive electrode, and a rechargeable lithium battery including the positive electrode are disclosed. The positive electrode active material includes a first positive electrode active material including a core particle in a form of secondary particles including a layered lithium nickel-manganese-based composite oxide and provided by agglomerating a plurality of primary particles and a second positive electrode active material including a core particle including a layered lithium nickel-manganese-based composite oxide and in a form of single particles. The first positive electrode active material and the second positive electrode active material each independently further include an aluminium coating layer on the surface of the core particle, and an average particle diameter (D50) of the second positive electrode active material is smaller than that of the first positive electrode active material.