ALD Apparatus Thermal Gradient Control for Precursor Delivery

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Solution Overview

Problem

In atomic layer deposition, maintaining a consistent temperature gradient along the supply path of low vapor pressure precursors is challenging, leading to potential condensation and deterioration of the deposition process due to temperature fluctuations.

Innovation Solution

The apparatus features a vacuum chamber positioned between precursor sources of different temperatures, with short supply channels and lead-through connections that minimize distance to the deposition chamber, ensuring optimal thermal conditions and preventing cold spots by using a heated vacuum chamber and separate compartments for high and low temperature precursors.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If precursor sources are arranged further away from the deposition chamber through long channels, then the apparatus structure is more flexible, but the temperature gradient cannot be maintained and precursor material condenses

Engineering Contradiction:
Improvetemperature gradientVSAvoidsupply channel length
Core Design Contradiction:
TemperatureVSLength of stationary object

Solution Approach 1:

The apparatus divides precursor supply into separate high-temperature and low-temperature precursor source arrangements positioned on opposite sides of the vacuum chamber. Each precursor source has its own dedicated supply channel, allowing independent temperature control and maintaining appropriate temperature gradients for different precursor materials without requiring a single long channel.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The precursor sources are arranged in different spatial dimensions - high-temperature sources on one side and low-temperature sources on the opposite side of the vacuum chamber. This spatial separation allows multiple precursor materials to be supplied simultaneously or sequentially while maintaining their respective temperature requirements, effectively using the third dimension to resolve the temperature-gradient conflict.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Productivity

If precursor materials are heated to maintain vapor pressure, then dosing speed is sufficient, but temperature fluctuations cause local condensation

Engineering Contradiction:
Improvedosing speedVSAvoidprocess stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

Different regions of the apparatus are assigned different thermal characteristics - high-temperature precursor sources for precursors requiring high vapor pressure and dosing speed, and low-temperature precursor sources for precursors that condense easily. Each precursor supply path has localized temperature control optimized for that specific precursor material, ensuring both adequate dosing speed and process stability without unwanted condensation.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration maintains the high temperature of heated precursors, preventing condensation and ensuring efficient precursor delivery to the deposition chamber, thereby enhancing the atomic layer deposition process by maintaining a consistent temperature gradient and preventing cold spots.

Implementation Method 1

maintaining an increasing temperature gradient along the supply path of the precursor material

Methodology Applied
Scientific EffectTemperature gradient: Temperature Gradient

Implementation Method 2

the gaseous precursor tends to condensate into liquid

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

the solid or liquid precursor materials are vaporized and dosed in gaseous form

Methodology Applied
Scientific EffectVaporization: Evaporation

Data Source

PatentUS11634814B2Atomic layer deposition apparatus
Publication Date: 2023.04.25 BENEQ OY
  • US11634814B2 patent drawing
  • US11634814B2 patent drawing
  • US11634814B2 patent drawing

AI summary

An atomic layer deposition apparatus having a vacuum chamber, a deposition chamber within the vacuum chamber, an inlet channel extending from outside of the vacuum chamber to the deposition chamber such that the inlet channel is connected to the deposition chamber for supplying gases to the deposition chamber, a discharge channel extending from the deposition chamber to outside of the vacuum chamber for discharging gases from the deposition chamber, one or more first precursor supply sources connected to the inlet channel, and one or more second precursor supply sources connected to the inlet channel. The vacuum chamber is arranged between the one or more first precursor supply sources and the one or more second precursor supply sources.