ALD Pulsing Valve With Continuous Purge to Prevent Particle Formation

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Solution Overview

Problem

Conventional atomic layer deposition (ALD) reactors face challenges in preventing precursor gas mixing, leading to particle formation and substrate damage, due to long purge times and potential trapping of precursor chemicals in valve cavities, which hinder high pulsing speed and chemical stability.

Innovation Solution

An apparatus with a pulsing valve featuring a closure and an additional cleaning chemical inlet to purge the valve output surface, ensuring continuous cleaning and preventing precursor chemical trapping, allowing for high pulsing speed and minimizing particle formation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a 4-way valve with vertical cavity is used for continuous purge gas flow, then continuous purging is achieved, but precursor chemicals are trapped in the cavity and cause particle formation on substrate

Engineering Contradiction:
Improvecontinuous purging capabilityVSAvoidparticle formation on substrate
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent extracts the harmful vertical cavity from the valve design by using a flat membrane closure that eliminates the cavity space where precursor chemicals could be trapped. The membrane provides a flat sealing surface that prevents chemical accumulation while maintaining the continuous purging function.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent introduces a flat membrane as an intermediary closure element that separates the purge gas flow path from the reaction chamber without creating trapped spaces. The membrane acts as a mediator that allows continuous purging while preventing precursor chemical trapping that would occur with traditional valve designs.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If long purge times are used to prevent gas mixing, then precursor chemical mixing is prevented, but process time increases and precursor chemicals decompose

Engineering Contradiction:
Improveprecursor gas separationVSAvoidprocess time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The patent implements continuous purging action through the flat membrane valve design that allows uninterrupted purge gas flow. This continuous action maintains precise gas separation without requiring extended purge times, enabling faster cycling while preventing precursor mixing and decomposition.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The patent uses rapid periodic pulsing of precursor gases separated by continuous purge cycles. The flat membrane valve enables this periodic action by quickly switching between precursor delivery and purging phases, maintaining gas separation while reducing overall process time and preventing chemical decomposition.

Inventive Principle:
Principle #19Periodic action

3Productivity

If high pulsing speed is implemented, then productivity increases, but precursor chemicals may be trapped in valve cavity causing particle formation

Engineering Contradiction:
Improvepulsing speedVSAvoidparticle formation on substrate
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The patent removes the vertical cavity from the valve design to eliminate the source of precursor chemical trapping. This extraction enables high pulsing speeds without the risk of chemicals being trapped and later released as particles on the substrate.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The flat membrane valve design performs preliminary purging action before each precursor pulse, ensuring no chemicals are trapped in the valve structure. This preliminary action prevents particle formation while enabling rapid pulsing cycles for high productivity.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution effectively prevents precursor chemical trapping and particle formation, enabling high-speed pulsing operations while maintaining substrate quality by continuously purging the valve output surface with a cleaning chemical, thus enhancing the efficiency and reliability of ALD processes.

Implementation Method 1

an additional cleaning chemical inlet at the reaction chamber side of the closure to purge the closure

Methodology Applied
Scientific EffectGas flow:

Implementation Method 2

a closure having an open and closed configuration to open and close, respectively, a route from the reactive chemical inlet to the reaction chamber outlet

Methodology Applied
Scientific EffectPhysical barrier:

Data Source

PatentUS11761082B2ALD apparatus, method and valve
Publication Date: 2023.09.19 PICOSUN OY
  • US11761082B2 patent drawing
  • US11761082B2 patent drawing
  • US11761082B2 patent drawing

AI summary

An apparatus, a method and a valve with a reactive chemical inlet, a reaction chamber outlet, and a closure having an open and closed configuration to open and close, respectively, a route from the reactive chemical inlet to the reaction chamber outlet, the valve further including an additional cleaning chemical inlet at a downstream side of the closure to purge the closure.