Aligned Carbon Nanotube Manufacturing via Solid Solvent Extrusion

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Solution Overview

Problem

The production of high-quality carbon nanotube articles is hindered by the inconsistency and cost inefficiency of existing methods, which fail to consistently produce materials with desirable mechanical and electrical properties.

Innovation Solution

A system and method involving the blending of unaligned carbon nanotube materials with solid solvent particles, activation of the solvent, and subsequent extrusion and solidification to produce aligned carbon nanotube products, utilizing a modular approach that includes solid state blending, homogenization, extrusion, and solidification modules to achieve high-purity and aligned carbon nanotube products.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional methods are used to produce carbon nanotube articles, then production can proceed with existing processes, but the quality consistency and mechanical properties of the products deteriorate

Engineering Contradiction:
Improvequality consistencyVSAvoidmechanical properties
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The patent transforms the solvent from liquid to solid state (parameter change in physical state) to enable precise control of nanotube dispersion and alignment. This parameter change allows the nanotubes to be uniformly distributed in the solid solvent, then aligned during extrusion, and finally fixed in the aligned state upon solvent solidification, thereby achieving both quality consistency and reliable mechanical properties

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The solid solvent acts as an intermediary medium between the unaligned carbon nanotube powder and the final aligned product. It temporarily holds the nanotubes in a controlled state, enabling uniform mixing and subsequent alignment during the phase transition process, which conventional liquid solvents or direct processing methods cannot achieve

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If existing production methods are used, then current manufacturing capabilities are maintained, but production cost efficiency deteriorates

Engineering Contradiction:
Improveproduction efficiencyVSAvoidproduction cost
Core Design Contradiction:
ProductivityVSEase of manufacture

Solution Approach 1:

The patent utilizes phase transitions of the solvent (liquid→solid during mixing, then solid→liquid during extrusion, and finally liquid→solid during product formation) to control the nanotube alignment process. This phase transition approach eliminates the need for complex alignment equipment and multiple processing steps, thereby reducing production costs while maintaining high productivity and efficiency

Inventive Principle:
Principle #36Phase transitions

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enables the production of high-strength, high-purity aligned carbon nanotube products with enhanced mechanical and electrical properties, such as tensile strength and electrical conductivity, while reducing production costs and improving efficiency.

Implementation Method 1

activating a nanotube solvent by liquefying the solid solvent particles

Methodology Applied
Scientific EffectLiquefaction: Melting

Implementation Method 2

forming a carbon nanotube proto-product by extruding the nanotube dope solution

Methodology Applied
Scientific EffectExtrusion: Extrusion

Implementation Method 3

forming an aligned carbon nanotube product by solidifying the carbon nanotube proto-product

Methodology Applied
Scientific EffectSolidification: Freezing

Data Source

PatentUS11667529B2Carbon nanotube product manufacturing system and method of manufacture thereof
Publication Date: 2023.06.06 WOOTZ LLC
  • US11667529B2 patent drawing
  • US11667529B2 patent drawing
  • US11667529B2 patent drawing

AI summary

A method of manufacturing a carbon nanotube product comprising: blending an unaligned carbon nanotube material with solid solvent particles; activating a nanotube solvent by liquefying the solid solvent particles; producing a nanotube dope solution by mixing the nanotube solvent and the unaligned carbon nanotube material; forming a carbon nanotube proto-product by extruding the nanotube dope solution; and forming an aligned carbon nanotube product by solidifying the carbon nanotube proto-product.