Alkaline Cation Conductive Ceramic Membrane Coating

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Solution Overview

Problem

Rechargeable metal-air batteries face limitations in mass energy density due to the reactivity of metallic lithium or sodium with water, leading to a significant increase in cationic resistance at the solid electrolyte/aqueous electrolyte interface, where a dense crystalline layer of alkali metal hydroxide forms, hindering conductivity.

Innovation Solution

A ceramic membrane conductive to alkaline cations is coated with a thin layer of an insoluble and chemically stable cation-conductive organic polymer, preventing the formation of a dense crystalline layer of alkali metal hydroxide at the interface, thereby maintaining high conductivity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a ceramic membrane conductive to alkaline cations is used to separate metallic lithium or sodium from aqueous electrolyte, then the reactivity between metal and water is prevented, but a dense crystalline layer of alkali metal hydroxide forms at the interface, significantly increasing cationic resistance

Engineering Contradiction:
Improveprevention of metal-water reactionVSAvoidcationic resistance increase
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

A thin layer of hydrophobic organic polymer is introduced as an intermediary between the ceramic membrane and the aqueous electrolyte. This polymer layer prevents direct contact between the aqueous environment and the ceramic surface, thereby preventing the formation of the dense crystalline hydroxide layer that causes high resistance, while still allowing cationic conduction to occur through the polymer matrix.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention changes the chemical and physical parameters at the interface by coating the ceramic membrane with a hydrophobic polymer. This modification alters the surface properties from hydrophilic to hydrophobic, preventing water and hydroxide crystallization while maintaining cationic conductivity through the modified interface structure.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If the concentration of alkali metal hydroxide in the aqueous electrolyte is increased to improve mass energy density, then the battery capacity increases, but precipitation of metal hydroxide occurs, limiting further concentration increase

Engineering Contradiction:
Improvealkali metal hydroxide concentrationVSAvoidprecipitation of metal hydroxide
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The hydrophobic polymer layer acts as a barrier that prevents the precipitation of metal hydroxide at the ceramic membrane interface. By blocking the interface where crystallization normally occurs, the polymer allows much higher concentrations of alkali metal hydroxide to be maintained in the aqueous electrolyte without precipitation, thereby enabling higher mass energy density.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Object-affected harmful factors

If a thin layer of hydrophobic organic polymer is coated on the ceramic membrane surface, then the formation of dense crystalline hydroxide layer is prevented and cationic conductivity is maintained, but the device complexity increases

Engineering Contradiction:
Improvecationic resistanceVSAvoidmembrane structure complexity
Core Design Contradiction:
Object-affected harmful factorsVSDevice complexity

Solution Approach 1:

A thin film of hydrophobic organic polymer is applied to the ceramic membrane surface. This thin film coating approach maintains the structural integrity and functionality of the original ceramic membrane while adding only a minimal layer that provides the necessary hydrophobic protection. The simplicity of the thin film application process helps minimize the increase in device complexity.

Inventive Principle:
Principle #30Flexible shells and thin films

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration enhances the cationic conductivity and prevents the undesirable crystallization of alkali metal hydroxide, improving the energy efficiency and lifespan of rechargeable metal-air batteries by maintaining low resistance and allowing for higher alkali metal hydroxide concentrations without precipitation issues.

Implementation Method 1

a membrane of solid electrolyte conducting alkaline cations

Methodology Applied
Scientific EffectCation conduction: Conduction (electrical)

Implementation Method 2

a thin layer of an insoluble and chemically stable cation-conductive organic polymer... which is hydrophobic

Methodology Applied
Scientific EffectHydrophobic effect: Hydrophobe

Data Source

PatentEP2494638B1Alcaline cation conductive ceramic membrane
Publication Date: 2016.05.04 ELECTRICITE DE FRANCE
  • EP2494638B1 patent drawingFigure 1
  • EP2494638B1 patent drawingFigure 2
  • EP2494638B1 patent drawing

AI summary

The present invention relates to an alkaline cation-conducting ceramic membrane covered, over at least a portion of the surface thereof, with a cation-conducting organic polyelectrolyte layer that is insoluble and chemically stable in pH-basic water. The invention also relates to an electrochemical device including such a membrane as a solid electrolyte in contact with a liquid electrolyte formed of an alkali metal hydroxide aqueous solution.