Alkaline Battery Positive Electrode Material Stabilization

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Solution Overview

Problem

Alkaline storage batteries face limitations in increasing the number of reaction electrons and discharge capacity due to low conductivity of Ni(OH)2 and instability of α-Ni(OH)2 in alkaline media, despite efforts to enhance Ni use efficiency and phase stabilization.

Innovation Solution

Incorporating a Sr compound, Ca compound, or lanthanide elements like Y and Lu into nickel hydroxide, with Al or Ga in solid solution, to stabilize α-phase and β-phase nickel hydroxide, thereby increasing the number of reaction electrons and discharge capacity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If Al is dissolved in solid solution in nickel hydroxide to stabilize α-phase, then the stability of α-Ni(OH)2 is improved, but the conductivity of the positive active material deteriorates

Engineering Contradiction:
Improvestability of α-Ni(OH)2VSAvoidconductivity of positive active material
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

The patent combines nickel hydroxide with cobalt oxyhydroxide coating and multiple dopant elements (Al, Ga, Y, lanthanides, Sr, Ca) to create a composite material structure. The CoOOH coating layer compensates for the low conductivity of Ni(OH)2 while the dopants stabilize the α-phase, achieving both stability improvement and conductivity maintenance through material composition design.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent optimizes the concentration parameters of dopant elements in nickel hydroxide. Specifically, Al or Ga is held in solid solution at 5-16 mol%, Y or lanthanide elements are present at 0.25-6 mass%, and Sr or Ca compounds are included at controlled amounts. These parameter optimizations balance phase stabilization with conductivity preservation.

Inventive Principle:
Principle #35Parameter changes

2Stability of the object's composition

If the content of A element (Al or Ga) in solid solution is increased to stabilize α-phase, then the stability of nickel hydroxide is improved, but the tap density of the material deteriorates

Engineering Contradiction:
Improvestability of nickel hydroxideVSAvoidtap density
Core Design Contradiction:
Stability of the object's compositionVSVolume of stationary object

Solution Approach 1:

The patent identifies an optimal parameter range for A element content at 5-16 mol% in solid solution. This optimized concentration provides sufficient α-phase stabilization while minimizing the negative impact on tap density, representing a balanced parameter optimization rather than extreme values.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite structure with multiple functional components: A element (Al/Ga) for phase stabilization, Y/lanthanide elements for enhancing reaction electrons, and Sr/Ca compounds for additional stabilization. This multi-component composite achieves phase stability with reduced adverse effects on physical properties like tap density compared to single-dopant systems.

Inventive Principle:
Principle #40Composite materials

3Quantity of substance

If Y or lanthanide elements are added to increase the number of reaction electrons, then the discharge capacity is improved, but the complexity of the positive electrode material increases

Engineering Contradiction:
Improvenumber of reaction electronsVSAvoidcomplexity of positive electrode material
Core Design Contradiction:
Quantity of substanceVSDevice complexity

Solution Approach 1:

The patent merges multiple functional elements into a single integrated positive electrode material system. Y or lanthanide elements (0.25-6 mass%), A elements (5-16 mol%), and Sr/Ca compounds are combined in one material formulation, allowing simultaneous achievement of phase stabilization, conductivity improvement, and enhanced reaction electron capacity without requiring separate components.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The positive electrode material is designed with multi-functionality: the A element (Al/Ga) provides phase stabilization, Y/lanthanide elements enhance the number of reaction electrons, and Sr/Ca compounds provide additional stabilization. This universal material design achieves multiple objectives within a single electrode composition, reducing overall system complexity.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The incorporation of these elements significantly enhances the number of reaction electrons and discharge capacity, with optimal results achieved when Al or Ga is in 5-16 mol% solid solution and lanthanide content is 0.25-6 mass%, particularly with Y, Sm to Lu, and Ca or Sr compounds, improving tap density and oxygen generation potential.

Implementation Method 1

an A element as at least one element selected from the group consisting of Al, and Ga is held in solid solution in a crystallite of the nickel hydroxide

Methodology Applied
Scientific EffectSolid solution: Solid Solution Strengthening

Data Source

PatentEP2713428B1Alkaline storage battery and positive electrode material for alkaline storage battery
Publication Date: 2017.01.11 GS YUASA INT LTD
  • EP2713428B1 patent drawingFigure 1~2
  • EP2713428B1 patent drawingFigure 3~4
  • EP2713428B1 patent drawingFigure 5~6

AI summary

A positive electrode material for an alkaline storage battery includes: nickel hydroxide; and at least one of a Sr compound, a Ca compound, and a compound of at least one element selected from the group consisting of Y and lanthanide elements of atomic number 62 (Sm) to 71 (Lu). An A element which is at least one element selected from the group consisting of Al, Ga, Mn, and Mo is held in solid solution in a crystallite of the nickel hydroxide. The content of the A element, [A]/([Ni] + [A]), is 5% or more and 16% or less (where [A] represents the molarity of the A element in the crystallite and [Ni] represents the molarity of Ni). The nickel hydroxide includes α-phase nickel hydroxide and β-phase nickel hydroxide. In this positive electrode material, the number of reaction electrons is large and moreover the capacity per volume is large.