Alkoxysilane Coating Composition for Metal Substrates

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Solution Overview

Problem

Current surface-protective coating compositions derived from alkoxysilanes face challenges in storage stability, adhesion, flexibility, corrosion resistance, abrasion/wear resistance, and optical clarity, particularly in the absence of chromium and heavy metals, which are toxic and environmentally harmful.

Innovation Solution

A curable surface-protective coating composition comprising specific alkoxysilanes, metal oxides, water-miscible organic solvents, acid hydrolysis catalysts, and optional condensation catalysts, formulated to achieve a viscosity range of 3.0 to 7.0 cStks, which is applied and cured to provide enhanced properties such as corrosion and abrasion resistance, adhesion, and optical clarity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If chromium and heavy metal phosphate conversion coatings are used to prepare metal surfaces, then corrosion resistance and adhesion are improved, but environmental pollution and toxicity increase

Engineering Contradiction:
Improvecorrosion resistanceVSAvoidenvironmental pollution
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The invention changes the chemical composition parameters by using alkoxysilane-based coatings with specific molecular structures (Formulas A and B) containing organofunctional groups, replacing toxic chromium and heavy metal phosphates. This parameter change maintains protective functionality while eliminating environmental harm.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite coating system combining alkoxysilane polymers with metal oxide particles (5-50 weight percent), forming a composite material that provides both corrosion protection and environmental safety. The composite structure integrates the protective properties of silane-based coatings with the beneficial characteristics of metal oxides.

Inventive Principle:
Principle #40Composite materials

2Object-affected harmful factors

If non-chromium, non-phosphate, and non-heavy metal based coating compositions are used, then environmental safety is improved, but storage stability and adhesion properties deteriorate

Engineering Contradiction:
Improveenvironmental safetyVSAvoidadhesion
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The invention optimizes chemical composition parameters by incorporating specific organofunctional groups (mercapto, acyloxy, glycidoxy, epoxy, epoxycyclohexyl, epoxycyclohexylethyl, hydroxy, episulfide, acrylate, methacrylate, ureido, thioureido, vinyl, allyl, —NHCOOR4, —NHCOSR4) into the alkoxysilane structure. These functional groups enhance adhesion to metal substrates while maintaining environmental safety.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention develops a composite formulation integrating alkoxysilane polymers with metal oxide particles and water-miscible organic solvents. This composite structure provides both environmental safety and improved adhesion properties through the synergistic interaction of its components.

Inventive Principle:
Principle #40Composite materials

3Object-affected harmful factors

If curable coating compositions derived from alkoxysilanes are used, then environmental safety is improved, but storage stability and cured coating properties (adhesion, flexibility, corrosion resistance, abrasion/wear resistance, optical clarity) require improvement

Engineering Contradiction:
Improveenvironmental safetyVSAvoidcomprehensive coating performance
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The invention creates a multi-component composite system comprising alkoxysilane polymers (Formulas A and B), metal oxide particles (5-50 weight percent), water-miscible organic solvents, acid hydrolysis catalysts, and optional condensation catalysts. This composite formulation simultaneously addresses storage stability and enhances cured coating properties including adhesion, flexibility, corrosion resistance, abrasion/wear resistance, and optical clarity.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention optimizes multiple parameters including the specific molecular structure of alkoxysilanes with defined carbon atom ranges (1-12, preferably 1-8), metal oxide content (5-50 weight percent), and viscosity control (3.0-7.0 cStks at 25°C). These parameter optimizations ensure both storage stability and superior cured coating performance.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composition exhibits excellent storage stability and cured coatings with high corrosion and abrasion resistance, good adhesion, flexibility, and optical clarity, making it suitable for metal surfaces while avoiding the use of toxic materials.

Implementation Method 1

at least one acid hydrolysis catalyst

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 2

curable coating compositions derived from alkoxysilanes

Methodology Applied
Scientific EffectCondensation: Condensation

Data Source

PatentUS11939490B2Curable surface-protective coating composition, processes for its preparation and application to a metallic substrate and resulting coated metallic substrate
Publication Date: 2024.03.26 MOMENTIVE PERFORMANCE MATERIALS INC

AI summary

A surface-protective coating forming composition exhibiting excellent shelf life (storage stability) and cured coating performance is derived from trialkoxysilane and metal oxide powder.