AlN Single Crystal Substrate Defect Density Control

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Solution Overview

Problem

AlN single crystal substrates used for deep ultraviolet light emitting elements often suffer from cracks during post-processing due to uneven dislocation density distribution, leading to reduced luminous efficiency and poor yield.

Innovation Solution

An AlN single crystal substrate with a three-layer structure is developed, where the defect density of the inside layer is higher than that of the front and back surfaces, effectively controlling the distribution of defects to suppress cracking.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If the dislocation density is reduced uniformly across the AlN single crystal substrate, then the defect density decreases, but cracks are more likely to occur during post-processing

Engineering Contradiction:
Improvedefect densityVSAvoidcrack resistance
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The patent applies local quality by creating a non-uniform dislocation density distribution within the AlN single crystal substrate. Specifically, the substrate is designed to have a first region with lower dislocation density and a second region with higher dislocation density. This localized variation in defect density allows the substrate to maintain overall low defect levels while having specific regions that can accommodate stress and prevent crack propagation during post-processing operations.

Inventive Principle:
Principle #3Local quality

2Ease of manufacture

If the AlN single crystal substrate is grown using conventional methods, then the production process is simple, but the dislocation density distribution is uneven leading to cracks

Engineering Contradiction:
Improveproduction process complexityVSAvoiddislocation density distribution
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent applies preliminary action by controlling the dislocation density distribution during the crystal growth process itself. By adjusting growth parameters such as temperature gradient, pressure, and composition during the initial stages of AlN single crystal formation, the desired non-uniform dislocation density distribution is established before subsequent processing steps. This preliminary control of defect distribution prevents cracks during post-processing without requiring complex additional manufacturing steps.

Inventive Principle:
Principle #10Preliminary action

Data Source

PatentUS20230392290A1AlN SINGLE CRYSTAL SUBSTRATE
Publication Date: 2023.12.07 NGK INSULATORS LTD
  • US20230392290A1 patent drawing
  • US20230392290A1 patent drawing
  • US20230392290A1 patent drawing

AI summary

Provided is an AlN single crystal substrate having a three-layer structure composed of one AlN single crystal as a whole and is classifiable into the first layer, the second layer, and the third layer in this order in the thickness direction in terms of defect density, wherein the second layer has a defect density of 10 times or more the defect density of each of the first layer and the third layer.