Alternating Graphene Oxide Boron Nitride Separator for Lithium-Sulfur Batteries

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Solution Overview

Problem

Lithium-sulfur batteries face issues with lithium polysulfides causing capacity loss and lithium dendrites leading to instability, safety concerns, and reduced lifespan due to the formation of lithium polysulfides and dendrites during charging and discharging.

Innovation Solution

A separator with a multi-layered coating layer composed of alternately laminated graphene oxide and boron nitride layers is used, which effectively adsorbs lithium polysulfides and inhibits the growth of lithium dendrites, enhancing the battery's capacity and stability by facilitating ion transfer while maintaining high sulfur loading.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a protective film is formed on the electrode to prevent lithium dendrite growth, then safety is improved, but the protective film acts as a resistive layer that lengthens or blocks the lithium ion path, reducing battery performance

Engineering Contradiction:
ImprovesafetyVSAvoidbattery performance
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The separator uses a porous structure with controlled pore size and distribution that allows lithium ions to pass through efficiently while providing physical barriers to dendrite growth. The porous architecture maintains ion conductivity pathways without requiring additional protective films that would block ion transport.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The separator combines multiple materials with complementary properties: a base separator material providing structural support and ion conductivity, combined with functional coatings or composite structures that enhance dendrite resistance while maintaining porosity for ion transport. This composite approach achieves both safety and performance.

Inventive Principle:
Principle #40Composite materials

2Loss of substance

If metal chalcogenide or alumina is added to delay sulfur leakage, then positive electrode active material retention is improved, but sulfur is lost during processing and the method is complicated, limiting the amount of active material that can be loaded

Engineering Contradiction:
Improvesulfur retentionVSAvoidprocessing complexity
Core Design Contradiction:
Loss of substanceVSDevice complexity

Solution Approach 1:

Instead of uniformly distributing sulfur-retention additives throughout the entire electrode, the invention applies functional materials locally at specific interfaces where sulfur leakage occurs most, such as coating the separator surface or creating localized functional layers. This reduces processing complexity and sulfur loss while maintaining effective retention.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The separator acts as an intermediary layer between the positive and negative electrodes, incorporating functional materials that specifically address sulfur leakage at the interface. This mediator approach prevents sulfur loss without requiring complex processing of the entire electrode structure, enabling higher sulfur loading.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Loss of substance

If the separator structure is enhanced to prevent lithium polysulfide diffusion, then capacity retention is improved, but ion transfer resistance increases, reducing charging/discharging efficiency

Engineering Contradiction:
Improvecapacity retentionVSAvoidcharging/discharging efficiency
Core Design Contradiction:
Loss of substanceVSProductivity

Solution Approach 1:

The separator is divided into multiple functional layers, each with specific properties: one layer provides polysulfide barrier functionality while another layer maintains high ion conductivity. This segmented structure allows simultaneous achievement of capacity retention and fast ion transport without compromising either function.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution improves the charging and discharging efficiency, extends the battery's life, and prevents short-circuiting, heat generation, and explosion risks, resulting in a more stable and high-capacity lithium-sulfur battery.

Implementation Method 1

a multi-layered coating layer formed by alternately laminating a graphene oxide layer and a boron nitride layer

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

the multi-layered coating layer is formed by alternately laminating a graphene oxide layer and a boron nitride layer

Methodology Applied
Scientific EffectIon conduction: Conduction (electrical)

Implementation Method 3

the separator comprises a porous substrate and a multi-layered coating layer formed on at least one side of the porous substrate

Methodology Applied
Scientific EffectPhysical barrier: Physical Containment

Data Source

PatentEP3460875B1Separator and lithium-sulfur battery comprising same
Publication Date: 2021.07.14 LG ENERGY SOLUTION LTD
  • EP3460875B1 patent drawingFigure 1
  • EP3460875B1 patent drawingFigure 2
  • EP3460875B1 patent drawingFigure 3

AI summary

The present invention relates to a separator capable of simultaneously solving the problems caused by the lithium polysulfides and lithium dendrites generated in a conventional lithium-sulfur battery wherein the separator includes a porous substrate alternately laminated with a graphene oxide layer and a boron nitride layer on its at least one side, and to a lithium-sulfur battery comprising the same.