Aluminium Alloy Powder Atomization for Grain Size and Oxidation Control

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Solution Overview

Problem

Existing methods for producing metal powders for additive manufacturing lack the ability to achieve a defined size distribution of grains, which is crucial for applications in sensitive industries like aircraft and automotive, and are prone to oxidation during production.

Innovation Solution

A method involving the gasification of a molten aluminum alloy using preheated primary and secondary inert gases, combined with a controlled atomization process in a spray tower, and subsequent classification to achieve a defined grain size distribution, while minimizing oxidation through inert atmospheres and cooling.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional atomization methods are used to produce metal powder, then production efficiency is maintained, but the grain size distribution becomes uncontrolled and oxidation occurs

Engineering Contradiction:
Improvegrain size distributionVSAvoidproduction process complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The production process is segmented into distinct functional zones: a first furnace chamber for melting and alloying, a second furnace chamber for atomization, and a spray tower for cooling. This segmentation allows each zone to be optimized independently for its specific function, achieving precise grain size control without overwhelming complexity

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

An inert gas atmosphere serves as an intermediary medium throughout the process, protecting the molten metal and powder from oxidation. The inert gas is introduced in both furnace chambers and maintained throughout the spray tower, creating a protective environment that prevents harmful chemical reactions while enabling precise process control

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If the melt is atomized without preheating the primary gas, then energy consumption is reduced, but oxidation occurs and grain formation is irregular

Engineering Contradiction:
Improveoxidation resistanceVSAvoidenergy consumption
Core Design Contradiction:
ReliabilityVSUse of energy by moving object

Solution Approach 1:

The primary gas is preheated to between 100°C and 450°C before entering the atomization chamber. This preliminary heating action ensures the gas is at the optimal temperature to prevent oxidation and promote regular grain formation, while the heating is efficiently achieved through thermal contact with the heated tundish or spray nozzle

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The tundish or spray nozzle serves a dual function: it delivers the molten metal for atomization and simultaneously heats the primary gas through thermal contact. This self-service approach eliminates the need for separate gas heating equipment, reducing overall system complexity while maintaining reliable oxidation protection

Inventive Principle:
Principle #25Self-service

3Manufacturing precision

If a single furnace chamber is used for melting and atomization, then device complexity is reduced, but manufacturing precision of grain size distribution deteriorates

Engineering Contradiction:
Improvegrain size distributionVSAvoidfurnace chamber configuration
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The production process is segmented into distinct functional zones: a first furnace chamber for melting and alloying, a second furnace chamber for atomization, and a spray tower for cooling. This segmentation allows each zone to be optimized independently for its specific function, achieving precise grain size control without overwhelming complexity

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Each furnace chamber is equipped with specific local characteristics: the first chamber has melting and alloying capabilities, the second chamber has atomization nozzles and inert gas injection, and the spray tower has cooling capabilities. This local quality optimization ensures each zone performs its function with maximum efficiency, resulting in superior grain size distribution

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces metal powder with a precise and regular grain size distribution suitable for additive manufacturing, reducing oxidation risks and ensuring high-quality powder production.

Implementation Method 1

atomizing the melt by means of a primary gas, which is an inert gas and has a first gas flow

Methodology Applied
Scientific EffectAtomization:

Implementation Method 2

the heating of the primary gas is additionally carried out by thermal contact with the heated tundish or its spray nozzle

Methodology Applied
Scientific EffectThermal contact heating: Conduction (thermal)

Implementation Method 3

Cooling the melt during the atomization and solidification of the metal powder

Methodology Applied
Scientific EffectCooling and solidification: Cooling

Data Source

PatentEP3725439B1Production of a metal powder of an aluminium alloy for use as a material in additive production
Publication Date: 2025.07.30 RIMMER KARL
  • EP3725439B1 patent drawingFigure 1

AI summary

A process for producing a metal powder of an aluminum alloy for use as a material in additive manufacturing is shown, wherein the metal powder of the aluminum alloy is produced from aluminum or from an existing aluminum alloy (1) and at least one other metal (20), wherein the production process of the metal powder of the aluminum alloy comprises the following steps: - Melting and alloying the aluminum or the existing aluminum alloy (1) with the at least one other metal (20), wherein the temperature of the melt (21) is 500°C to 1400°C, preferably 1100°C to 1200°C, particularly preferably about 1150°C; - Atomizing the melt (21) by means of a primary gas which has a first gas flow, and wherein the primary gas is preheated to 100°C to 450°C;- Cooling of the melt (21) during atomization and solidification to form metal powder, wherein a material flow during atomization and solidification takes place in a spray tower (16), and wherein the melt (21) is introduced into a heated tundish (12) immediately before atomization, the tundish (12) having a spray nozzle (15) at a lower end and at least one supply line (14) for the primary gas and optionally the secondary gas, such that the heating of the primary gas and optionally the secondary gas is additionally effected by thermal contact with the heated tundish (12) or its spray nozzle (15).