Amine Catalyst for Polyurethane Reducing VOC Emissions

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Solution Overview

Problem

Conventional amines used as catalysts in polyurethane reactions often emit volatile organic compounds (VOCs) and odorous species, leading to issues like fogging and adverse health effects due to their volatility and reactivity.

Innovation Solution

Development of specific amines with the formula (CH3)2NCH2CH2OCH2CH2N(R1)(R2), where R1 and R2 can be various alkyl or hydroxyl groups, which act as catalysts in polyurethane reactions, reducing VOC emissions and odor by increasing molecular weight and lowering vapor pressure, thereby minimizing bonding within the polyurethane product.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional amines are used as catalysts in polyurethane reactions, then the catalytic activity is sufficient, but VOC emissions and odorous species increase

Engineering Contradiction:
Improvecatalytic activityVSAvoidVOC emissions and odorous species
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The patent changes the molecular weight parameter of the amine catalyst by introducing longer alkyl chains (n=0-5) and hydroxyl groups (m=2-4) in the general formula (CH3)2NCH2CH2OCH2CH2N(R1)(R2). This parameter change increases molecular weight while maintaining catalytic activity, thereby reducing volatility and VOC emissions.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates composite amine structures by combining dimethylamino groups with various alkyl and hydroxyl substituents in a specific molecular architecture. This composite structure achieves both sufficient catalytic activity and reduced volatility by distributing functional groups across a larger molecular framework.

Inventive Principle:
Principle #40Composite materials

2Object-generated harmful factors

If amine molecular weight is increased to reduce volatility, then VOC emissions decrease, but catalytic efficiency may be reduced

Engineering Contradiction:
ImproveVOC emissionsVSAvoidcatalytic efficiency
Core Design Contradiction:
Object-generated harmful factorsVSProductivity

Solution Approach 1:

The patent applies local quality by concentrating the catalytically active dimethylamino groups at specific locations in the molecular structure while extending the alkyl chains and adding hydroxyl groups at other positions. This spatial distribution maintains local catalytic activity while the overall molecular size reduces volatility.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent introduces dynamic flexibility through alkyl chains of variable length (n=0-5) and hydroxyl groups (m=2-4), allowing the molecular structure to adapt its conformation. This dynamic structure maintains catalytic effectiveness while the increased molecular weight and reduced flexibility overall decrease volatility.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The new amines effectively catalyze polyurethane reactions, reducing VOC emissions and offensive odors, as they are either reactive and bond within the product or non-reactive but still reduce volatility, outperforming conventional catalysts in terms of reduced vapor pressure and odor impact.

Implementation Method 1

Amines are well known as catalysts in the reaction of isocyanates with isocyanate reactive groups

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

reducing VOC emissions and odor by increasing molecular weight and lowering vapor pressure

Methodology Applied
Scientific EffectVapor pressure reduction: Vapour Pressure

Data Source

PatentEP2858973B1Amine suitable as PU-catalyst
Publication Date: 2018.10.31 HUNTSMAN PETROCHEMICAL LLC

AI summary

An amine according to the invention has a formula (CH3)2NCH2CH2OCH2CH2CH2N(R1)(R2) wherein R1 is selected from (CH3)2NCH2CH2OCH2CH2CH2- and R2 is selected from the group consisting of H-, CH3(CnH2n)-,HO(CmH2m)- and (CH3)2NCH2CH2OCH2CH2CH2-, n being an integer in the range of 0 to 5, m being an integer in the range of 2 to 4.