Ammonia-Modified SAPO-34 Catalyst for Ethylene Selectivity

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Solution Overview

Problem

Current processes for converting methanol to olefins, such as ethylene and propylene, face challenges in increasing the ratio of ethylene to propylene and overall selectivity, despite advancements in using oxygenate feeds and catalyst modifications.

Innovation Solution

Incorporating 0.05 to 0.5 weight percent ammonia in the methanol feed and employing SAPO molecular sieves or metal-substituted SAPO molecular sieves as catalysts to enhance the conversion process, specifically increasing the ethylene to propylene ratio by optimizing reaction conditions and catalyst selection.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional catalysts and processes are used for converting methanol to olefins, then overall olefin production is maintained, but the ratio of ethylene to propylene cannot be increased

Engineering Contradiction:
Improveethylene to propylene ratioVSAvoidoverall olefin production
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The patent applies parameter changes by introducing ammonia at specific concentrations (0.05-0.5 weight percent) into the methanol feedstock and optimizing reaction conditions such as temperature (250-450°C) and pressure (1-50 atm). This modifies the reaction parameters to shift product selectivity toward ethylene while maintaining overall olefin production levels through controlled catalytic conversion over SAPO-34 molecular sieve catalysts

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If catalyst composition is modified to increase ethylene selectivity, then ethylene to propylene ratio increases, but process complexity increases

Engineering Contradiction:
Improveethylene selectivityVSAvoidcatalyst composition complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent employs ammonia as an intermediary substance added to the methanol feedstock. This intermediary modifies the reaction environment and catalyst behavior to enhance ethylene selectivity without requiring complex catalyst formulations. The ammonia interacts with the SAPO-34 catalyst and reactants to promote ethylene formation pathways while keeping the catalyst composition relatively simple

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention changes the chemical composition parameter of the feedstock by introducing ammonia at controlled concentrations (0.05-0.5 weight percent). This parameter change affects the reaction mechanism and product distribution, achieving higher ethylene selectivity through feed modification rather than complex catalyst design

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly increases the ethylene to propylene ratio by up to 15 percent by weight, enhancing selectivity to ethylene by 2 to 4 percent by weight, while maintaining overall olefin production levels, even when the combined ethylene and propylene selectivity remains unchanged.

Implementation Method 1

The preferred process for converting an oxygenate feedstock, such as methanol or dimethyl ether (DME), into one or more olefins involves contacting the feedstock with a crystalline molecular sieve catalyst composition

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

from 0.05 to 0.5 weight percent of ammonia is included in the methanol feed, such that the ratio of ethylene to propylene in the product is increased

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentEP2552862B1Process to increase selectivity to ethylene in oxygenates-to-olefins conversions
Publication Date: 2015.09.09 DOW GLOBAL TECHNOLOGIES LLC

AI summary

A process for converting an oxygenate-containing feedstock to a product comprising olefins comprises including in the oxygenate-containing feedstock an amount of ammonia. The presence of the ammonia increases the product's ratio of ethylene to propylene.