Ammonia Vaporization Switching for Hydrogen Production Start-Up

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Traditional hydrogen production methods face challenges in efficiently vaporizing ammonia during the start-up phase due to insufficient heat from effluent gases, particularly in low-temperature flue gas ducts, leading to inefficiencies in energy usage and hydrogen production.

Innovation Solution

A process utilizing multiple heating media, including steam and cracked gas, to vaporize ammonia, with a heat exchanger system that integrates steam and effluent gas heat exchange to optimize energy use and enhance hydrogen production efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of energy

If waste heat from effluent gases is used to vaporize ammonia during normal operation, then energy efficiency is improved, but during start-up phase the flue gas temperature is too low to provide sufficient heat for vaporization

Engineering Contradiction:
Improveenergy efficiencyVSAvoidvaporization capability during start-up
Core Design Contradiction:
Loss of energyVSReliability

Solution Approach 1:

The patent introduces a preliminary heating stage using steam as the heating medium during the start-up phase, before the effluent gases reach sufficient temperature. This preliminary action ensures that ammonia vaporization can commence and continue smoothly until the waste heat recovery system becomes fully operational, thereby resolving the contradiction between energy efficiency and start-up reliability.

Inventive Principle:
Principle #10Preliminary action

2Device complexity

If a single heating medium is used for ammonia vaporization, then the system is simpler, but it cannot adapt to different operational phases (start-up vs. normal operation)

Engineering Contradiction:
Improveheating system complexityVSAvoidadaptability to operational phases
Core Design Contradiction:
Device complexityVSAdaptability or versatility

Solution Approach 1:

The patent implements a dynamic heating system that automatically switches between steam and effluent gases as the heating medium based on the operational phase. During start-up, steam is used; during normal operation, effluent gases take over. This dynamic adaptation resolves the contradiction by allowing the system to optimize for simplicity when possible while maintaining adaptability when needed.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The heating system is designed to perform multiple functions using different heating media for different operational conditions. The same vaporization system can utilize either steam or effluent gases depending on the phase of operation, making it universally applicable across all operational scenarios while maintaining relatively simple overall system architecture.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Ensures effective ammonia vaporization throughout different operational phases, including start-up, optimizing energy usage and enhancing hydrogen production efficiency, with the potential to produce a pure hydrogen stream exceeding 90 mol% hydrogen.

Implementation Method 1

sending at least part of the liquid phase of the ammonia stream from the vaporizer to a first heat exchanger arranged to at least partially vaporize said liquid phase by heat exchange with the effluent gas

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 2

vaporizing at least a portion of the ammonia stream, optionally by heating the ammonia stream with a heating medium

Methodology Applied
Scientific EffectVaporization: Evaporation

Implementation Method 3

optionally, performing a combustion to bring a heat input to the process

Methodology Applied
Scientific EffectCombustion: Combustion

Data Source

PatentEP4691969A1Process for producing a hydrogen product
Publication Date: 2026.02.11 LAIR LIQUIDE SA POUR LETUDE & LEXPLOITATION DES PROCEDES GEORGES CLAUDE
  • EP4691969A1 patent drawingFigure 1~2
  • EP4691969A1 patent drawingFigure 3
  • EP4691969A1 patent drawing

AI summary

A process (100) for producing a hydrogen product (20) from a feedstock stream (10), the process (100) comprising the following steps: - discharging an effluent gas stream from the gas conversion unit (S12), - providing heat from the effluent gas to contribute to vaporize the ammonia stream (10) of the vaporizer (5), - wherein vaporizing at least a portion of the ammonia stream (10) in said vaporizer (5) (S2) comprises heating said portion of the ammonia stream (10) with a heating medium different from the effluent gas, - the process (100) further comprising sending the vaporized ammonia (14) from said vaporizer (5) as said feedstock stream (10) and/or sending the vaporized ammonia (14) from said vaporizer (5) as a fuel to said combustion.