Amorphous Carbon Coating Adhesion via Chromium Silicon Sub-layer

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Solution Overview

Problem

Current methods for depositing tetrahedral amorphous carbon (ta-C) coatings require cooling and high-energy carbon ion bombardment, which can lead to overheating and electrical arcs, compromising adhesion and mechanical properties, especially in lubricated environments like automotive components.

Innovation Solution

A non-hydrogenated amorphous carbon coating with a sub-layer composed of chromium, carbon, and silicon, with specific atomic ratios, allowing for adhesion without cooling and at lower bias voltages, eliminating the need for high-energy ion bombardment and reducing the risk of overheating and electrical arcs.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If high-energy carbon ion bombardment is used to achieve adhesion, then adhesion strength is improved, but temperature increases causing overheating and electrical arcs

Engineering Contradiction:
Improveadhesion strengthVSAvoidsubstrate temperature
Core Design Contradiction:
StrengthVSTemperature

Solution Approach 1:

A sub-layer comprising chromium, carbon and silicon is introduced as an intermediary between the metal substrate and the ta-C coating. This sub-layer enables adhesion to be achieved at lower ion energies (reducing temperature rise) while maintaining bonding strength, thus mediating between the conflicting requirements of strong adhesion and temperature control.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention changes the energy parameter of ion bombardment from very high energy (kilo-electronvolts) to lower energy levels. By modifying this critical parameter and introducing the intermediate sub-layer, the system achieves sufficient adhesion without the excessive heating that would occur with high-energy bombardment alone.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If cooling steps are implemented before deposition, then adhesion quality is improved, but processing time increases

Engineering Contradiction:
Improveadhesion qualityVSAvoidcooling time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The sub-layer is deposited beforehand as a preparatory action that enables subsequent deposition to proceed without requiring cooling steps. This preliminary creation of the intermediate layer eliminates the need for time-consuming cooling procedures while ensuring adhesion quality is maintained.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The chromium-carbon-silicon sub-layer acts as a mediator that allows the deposition process to occur at higher temperatures without compromising adhesion. This intermediary layer eliminates the need for pre-cooling the substrate, thereby reducing processing time while maintaining reliability.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If high voltage is applied for ion acceleration, then deposition rate is improved, but electrical arcs occur destroying parts or adhesion

Engineering Contradiction:
Improvedeposition rateVSAvoidelectrical arcs
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The sub-layer serves as a protective intermediary that enables lower voltage operation. By introducing this intermediate chromium-carbon-silicon layer, the system can achieve adequate deposition rates without requiring the extremely high voltages that would otherwise trigger electrical arcs and damage the parts.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves stable and long-lasting adhesion of the DLC coating to the substrate, maintaining mechanical properties and preventing overheating, while ensuring reliable deposition without cooling steps or electrical arc risks.

Implementation Method 1

a sub-layer and with a coating of non-hydrogenated amorphous carbon, the latter being deposited on the sub-layer comprising chromium, carbon and silicon

Methodology Applied
Scientific EffectAdhesion: Adhesive

Implementation Method 2

They designate carbon-based materials generally obtained in the form of a thin layer and by vacuum deposition technologies

Methodology Applied
Scientific EffectVacuum deposition: Physical Vapour Deposition

Data Source

PatentUS11732343B2Part coated with a non-hydrogenated amorphous carbon coating on an undercoat comprising chromium, carbon and silicon
Publication Date: 2023.08.22 CENT STEPHANOIS DE RECH MECANIQUES HIDROMECANIQUE & FROTTEMENT

AI summary

Disclosed is a part comprising a metal substrate, a non-hydrogenated amorphous ta-C or aC carbon coating that coats the substrate, and an undercoat which is based on chromium (Cr), carbon (C) and silicon (Si) and is disposed between the metal substrate and the amorphous carbon coating and to which the amorphous carbon coating is applied, characterized in that the undercoat included, at its interface with the amorphous carbon coating, a ratio of silicon in atomic percent to chromium in atomic percent (Si/Cr) of 0.3 to 0.60, and a ratio of carbon in atomic percent to silicon in atomic percent (C/Si) of 2.5 to 3.5.