Amorphous Composite Metal Oxide Adsorbent for High-Temperature CO2 Capture

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Solution Overview

Problem

Current adsorbents for capturing carbon dioxide from flue gas at intermediate temperatures (150 to 400 °C) are complex and costly, requiring cooling or heating of flue gas, and lack high adsorption performance.

Innovation Solution

A composite metal oxide adsorbent with an amorphous structure, composed of a divalent first metal, a trivalent second metal, and an element with electronegativity between 2.0 and 4.0 on the Pauling scale, manufactured through a method involving pH adjustment, precipitation, ion exchange, and calcination, enhancing adsorption performance and thermal stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional adsorbents (MOF, zeolite, carbon) are used for low temperature CO2 capture, then adsorption performance is improved, but process complexity and additional costs increase due to required cooling or heating

Engineering Contradiction:
Improveadsorption performanceVSAvoidprocess complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The invention changes the operating temperature parameter by developing an adsorbent that functions effectively at ambient to moderately elevated temperatures (up to 400°C), eliminating the need for cooling or heating processes. This is achieved through selecting specific metal oxides (CaO, SrO, BaO, MgO) and controlling synthesis conditions to optimize surface properties for high-temperature CO2 adsorption.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses composite metal oxide materials combining divalent metals (Ca, Sr, Ba, Mg) with controlled surface properties. These composite structures provide both high CO2 adsorption capacity and thermal stability, replacing the need for complex temperature control systems while maintaining effective adsorption performance.

Inventive Principle:
Principle #40Composite materials

2Stability of the object's composition

If adsorbents are designed for high temperature operation, then thermal stability is improved, but adsorption performance decreases

Engineering Contradiction:
Improvethermal stabilityVSAvoidadsorption performance
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

The invention applies local quality by creating metal oxide adsorbents with specific surface characteristics (high surface area, controlled porosity, specific surface chemistry) that maintain high CO2 adsorption affinity even at elevated temperatures. The bulk material provides thermal stability while the surface properties enable effective adsorption, resolving the contradiction between thermal stability and adsorption performance.

Inventive Principle:
Principle #3Local quality

3Reliability

If flue gas is cooled to use low temperature adsorbents, then adsorption performance is improved, but energy consumption and process complexity increase

Engineering Contradiction:
Improveadsorption performanceVSAvoidenergy consumption
Core Design Contradiction:
ReliabilityVSUse of energy by moving object

Solution Approach 1:

The invention changes the temperature parameter from low temperature (requiring cooling) to ambient or moderately elevated temperatures where the metal oxide adsorbents naturally function. This eliminates energy-consuming cooling processes while maintaining high CO2 adsorption performance through the inherent properties of the metal oxide materials.

Inventive Principle:
Principle #35Parameter changes

4Stability of the object's composition

If conventional adsorbents require heating for high temperature operation, then thermal stability is improved, but process complexity and costs increase

Engineering Contradiction:
Improvethermal stabilityVSAvoidprocess complexity
Core Design Contradiction:
Stability of the object's compositionVSDevice complexity

Solution Approach 1:

The invention changes the operating temperature parameter to match the natural operating range of metal oxide adsorbents, which are inherently stable at ambient to moderately elevated temperatures. This eliminates the need for heating processes and associated equipment, simplifying the overall system while maintaining thermal stability and adsorption effectiveness.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composite metal oxide adsorbent demonstrates superior carbon dioxide adsorption capacity and thermal stability, maintaining high performance across a range of temperatures from 150 to 400 °C, with enhanced specific surface area and improved adsorption efficiency.

Implementation Method 1

an adsorbent having a relatively high adsorption performance is required

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

which has a relatively high adsorption performance and thermal stability and works at a relatively high temperature

Methodology Applied
Scientific EffectThermal stability:

Data Source

PatentEP2623197B1Method for manufacturing an adsorbent for carbon dioxide
Publication Date: 2019.09.04 SAMSUNG ELECTRONICS CO LTD
  • EP2623197B1 patent drawingFigure 1
  • EP2623197B1 patent drawingFigure 2
  • EP2623197B1 patent drawingFigure 3

AI summary

An adsorbent for carbon dioxide may include a composite metal oxide including a divalent first metal (M1), a trivalent second metal (M2), and an element (A) with an electronegativity of about 2.0 to about 4.0. The composite metal oxide may have an amorphous structure. A method of manufacturing the adsorbent for carbon dioxide and a capture module for carbon dioxide including the adsorbent for carbon dioxide are also disclosed.