Amorphous Copolymer Powder for Layer-by-Layer Molding

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Solution Overview

Problem

Current polymer powder-based layer-by-layer manufacturing processes face challenges such as curl distortion, non-uniform volume change due to crystallinity, high viscosity leading to porosity, and the inability to meet diverse material requirements like viscosity, thermal stability, and strength in a single component, limiting the precision and efficiency of rapid prototyping.

Innovation Solution

Development of a thermoplastic random copolymer powder with a melt flow rate (MFR) of 12 g/10 min to 1 g/10 min and a relative solution viscosity of 1.55 to 1.9, specifically a copolyamide with certain monomer units, which allows for selective melting via electromagnetic energy, reducing processing temperature and improving mechanical properties, processability, and reducing shrinkage.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If semicrystalline thermoplastics are used in layer-by-layer manufacturing, then the material provides good mechanical properties, but curl distortion occurs and volume change is non-uniform due to crystallinity

Engineering Contradiction:
Improvemechanical propertiesVSAvoidcurl distortion
Core Design Contradiction:
StrengthVSManufacturing precision

Solution Approach 1:

The patent changes the material parameter from semicrystalline to amorphous thermoplastic, fundamentally altering the phase behavior and eliminating crystallization-induced distortion while maintaining mechanical properties through controlled viscosity and molecular structure

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention exploits the phase transition characteristics of amorphous thermoplastics, which undergo glass transition rather than crystallization, thereby avoiding the non-uniform volume change and curl distortion associated with semicrystalline material phase changes

Inventive Principle:
Principle #36Phase transitions

2Manufacturing precision

If the construction chamber temperature is kept just below the melting point to avoid curl, then curl distortion is reduced, but the cooling period becomes significant and productivity decreases

Engineering Contradiction:
Improvecurl controlVSAvoidcooling period
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The patent changes the material's thermal parameters by selecting amorphous thermoplastics with specific glass transition temperatures and thermal conductivities, enabling faster cooling rates that reduce the cooling period while maintaining dimensional stability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention implements periodic layer deposition and cooling cycles optimized for amorphous materials, where each layer is rapidly cooled before the next is applied, reducing overall cooling time while preventing distortion through controlled thermal history

Inventive Principle:
Principle #19Periodic action

3Manufacturing precision

If amorphous thermoplastics with high viscosity are used, then curl distortion is reduced, but the material becomes porous due to inability to coalesce properly

Engineering Contradiction:
Improvedimensional stabilityVSAvoidporosity
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The patent optimizes the viscosity parameter by selecting amorphous thermoplastics with controlled molecular weight and chain structure, achieving a viscosity range that allows proper coalescence and densification while maintaining dimensional stability during processing

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses composite amorphous thermoplastic formulations combining different polymer components or additives that modify rheological behavior, enabling simultaneous achievement of low distortion and high density through improved melt flow and bonding characteristics

Inventive Principle:
Principle #40Composite materials

4Device complexity

If a single polymer material is used to meet diverse requirements, then material complexity is reduced, but it is impossible to simultaneously optimize viscosity, thermal stability, and strength

Engineering Contradiction:
Improvematerial compositionVSAvoidmaterial properties
Core Design Contradiction:
Device complexityVSAdaptability or versatility

Solution Approach 1:

The patent employs composite thermoplastic materials combining multiple polymer components, fillers, or functional additives in an amorphous matrix, enabling simultaneous optimization of viscosity, thermal stability, and mechanical strength while maintaining a relatively simple single-phase structure suitable for layer-by-layer manufacturing

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The copolymer powder enables faster and more reliable production of moldings with improved mechanical properties, reduced shrinkage, and increased processing latitude, while maintaining sharpness and precision, overcoming the limitations of conventional powders by allowing for tailored properties in a single component.

Implementation Method 1

regions of a powder layer are selectively melted via introduction of electromagnetic energy

Methodology Applied
Scientific EffectElectromagnetic energy absorption: Absorption (EM radiation)

Implementation Method 2

regions of a powder layer are selectively melted via introduction of electromagnetic energy

Methodology Applied
Scientific EffectMelting: Melting

Implementation Method 3

Once the previously molten regions have been cooled and hardened

Methodology Applied
Scientific EffectCooling: Cooling

Data Source

PatentUS7906063B2Process for producing moldings
Publication Date: 2011.03.15 EVONIK OPERATIONS GMBH

AI summary

The present invention is directed to a process of producing moldings by a layer-by-layer process including selectively melting regions of a respective pulverulent layer via unfocused introduction of electromagnetic energy, using a polymer powder, wherein the powder includes at least one thermoplastic random copolymer with an ISO 1133 MFR value of from 12 to 1 gm/10 min.