Amorphous Phosphate Layer for Piston Coating Adhesion

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Solution Overview

Problem

Existing methods for applying anti-friction coatings to steel pistons in internal combustion engines face challenges with adhesion due to insufficient surface preparation, leading to contamination and increased manufacturing costs, particularly with manual handling and conventional phosphating processes.

Innovation Solution

A method involving the formation of an amorphous phosphate layer through spraying a phosphoric acid solution onto the piston surface, which roughens and prepares the surface for better bonding of the anti-friction coating, and optionally followed by a manganese phosphate layer, allowing for improved adhesion and reduced contamination risks.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional manganese phosphating is applied via immersion process, then adhesion of sliding coating is improved, but manual handling causes surface contamination and increased manufacturing complexity

Engineering Contradiction:
Improveadhesion of sliding coatingVSAvoidmanual handling process
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent replaces manual mechanical handling with an automated spray application system. The phosphoric acid solution is applied through spraying technology, eliminating the need for manual immersion handling and reducing surface contamination while maintaining consistent coating quality

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The spray application system allows the piston surface to be treated automatically without manual intervention. The process is self-regulating with controlled spray parameters that ensure consistent phosphate layer formation without requiring operator skill or attention

Inventive Principle:
Principle #25Self-service

2Object-generated harmful factors

If neutral, alkaline, and/or acidic wash is applied before sliding coating, then surface degreasing is achieved, but adhesion remains inadequate due to lack of surface roughening

Engineering Contradiction:
Improvesurface greaseVSAvoidadhesion of sliding coating
Core Design Contradiction:
Object-generated harmful factorsVSReliability

Solution Approach 1:

The patent changes the chemical parameters of the treatment solution by using phosphoric acid with specific concentration ranges (4-14% g/g) and pH levels (1-3). This chemical parameter change enables simultaneous degreasing and surface roughening, creating an amorphous phosphate layer that provides both cleaning and anchoring functions

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite surface structure by forming an amorphous phosphate layer that combines the cleaning function with a roughened surface topology. This composite layer integrates both degreasing and mechanical anchoring properties in a single treatment step

Inventive Principle:
Principle #40Composite materials

3Object-affected harmful factors

If thick crystalline phosphate layer is applied, then surface protection is improved, but manufacturing tolerances become looser and coating precision decreases

Engineering Contradiction:
Improveoxidation protectionVSAvoidcoating thickness tolerance
Core Design Contradiction:
Object-affected harmful factorsVSManufacturing precision

Solution Approach 1:

The patent changes the structural parameters of the phosphate layer by controlling solution concentration, temperature (30-80°C), and treatment duration (50-500 seconds) to form a thin amorphous layer (0.05-3 μm) instead of thick crystalline structures, achieving both protection and precision

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates local quality differences by forming an amorphous phosphate layer with specific local properties - thin enough for precision (0.05-3 μm) but sufficiently protective through its amorphous structure and capillary network, providing localized optimization of both protection and tolerance

Inventive Principle:
Principle #3Local quality

4Area of stationary object

If manual immersion process is used for phosphating, then complete surface coverage is achieved, but production time increases and productivity decreases

Engineering Contradiction:
Improvesurface coverageVSAvoidmanufacturing cycle time
Core Design Contradiction:
Area of stationary objectVSProductivity

Solution Approach 1:

The patent replaces the slow manual immersion mechanical process with rapid spray application. The spray system covers the piston surface quickly and uniformly, dramatically reducing treatment time while maintaining complete surface coverage through controlled spray patterns

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The spray application process enables continuous treatment of piston surfaces without the interruption and handling time required by immersion methods. The process can be integrated into continuous manufacturing lines, maintaining productive action throughout the treatment cycle

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The amorphous phosphate layer enhances the anchoring of anti-friction coatings, ensuring better load-bearing capabilities and preventing oxidation, while being applied inline and with lower manufacturing tolerances, thus improving coating adhesion and reducing manufacturing expenses.

Implementation Method 1

the formation of an amorphous phosphate layer by spraying a solution containing phosphoric acid onto the piston surface

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 2

The treatment with the phosphoric acid-containing solution in step (1) not only forms an amorphous phosphate layer, but also roughens the piston surface and removes any existing oxides

Methodology Applied
Scientific EffectSurface roughening: Abrasion

Implementation Method 3

the amorphous phosphate layer acts as a passivation layer, thus preventing re-oxidation of the piston

Methodology Applied
Scientific EffectPassivation: Oxidation

Implementation Method 4

The amorphous phosphate layer formed according to the invention has capillaries and thus enables better anchoring of the sliding lacquer

Methodology Applied
Scientific EffectCapillary action: Capillary Action

Implementation Method 5

the phosphoric acid-containing solution is applied by spraying, enabling the amorphous phosphate layer to be produced inline

Methodology Applied
Scientific EffectSpray deposition: Spray

Data Source

PatentEP3619416B1Steel piston having a phosphate layer
Publication Date: 2021.10.13 FEDERAL MOGUL NURNBERG GMBH

AI summary

The invention relates to a steel piston for an internal combustion engine, comprising an amorphous phosphate layer in at least one region thereof. Said layer improves adhesion of a solid film lubricant.