Amorphous Sodium Solid Electrolyte for Low-Temperature Densification

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Solution Overview

Problem

Conventional beta-alumina-based solid electrolytes in all-solid-state sodium secondary batteries face issues with material compatibility during high-temperature firing, leading to deteriorated battery characteristics due to reactions between the electrode active material and the solid electrolyte.

Innovation Solution

A solid electrolyte composed of alkali metal oxide and silicon oxide, amorphous in nature, is used, allowing for excellent adhesion to the electrode and enabling densification at temperatures below 200°C, thereby maintaining good battery characteristics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If conventional beta-alumina-based solid electrolyte is fired at high temperatures to achieve excellent adhesion and dense electrode structure, then adhesion to electrode is improved and electrode density is improved, but material compatibility deteriorates due to reactions between electrode active material and solid electrolyte

Engineering Contradiction:
ImproveadhesionVSAvoidmaterial compatibility
Core Design Contradiction:
StrengthVSStability of the object's composition

Solution Approach 1:

The patent changes the firing temperature parameter from conventional high temperatures (typically above 900°C for beta-alumina) to low temperatures (below 400°C). This parameter change allows the solid electrolyte to achieve sufficient adhesion and densification without triggering harmful reactions between the electrode active material and the solid electrolyte, thus resolving the contradiction between adhesion strength and material compatibility.

Inventive Principle:
Principle #35Parameter changes

2Volume of stationary object

If conventional beta-alumina-based solid electrolyte is fired at high temperatures to achieve dense electrode structure, then electrode density is improved, but battery characteristics deteriorate due to material reactions

Engineering Contradiction:
Improveelectrode densityVSAvoidbattery characteristics
Core Design Contradiction:
Volume of stationary objectVSReliability

Solution Approach 1:

The patent applies low-temperature firing (below 400°C) instead of conventional high-temperature firing. This parameter change enables the solid electrolyte to achieve adequate densification for good battery performance without causing material reactions that would deteriorate battery characteristics, thus resolving the contradiction between electrode density and reliability.

Inventive Principle:
Principle #35Parameter changes

3Strength

If high-temperature firing is used to achieve excellent adhesion, then adhesion is improved, but choice of electrode active material is limited due to material reactions

Engineering Contradiction:
ImproveadhesionVSAvoidchoice of electrode active material
Core Design Contradiction:
StrengthVSAdaptability or versatility

Solution Approach 1:

By changing the firing temperature parameter to low temperatures (below 400°C), the patent eliminates thermal reaction constraints between the solid electrolyte and various electrode active materials. This enables broader material selection and greater versatility in electrode design while maintaining adequate adhesion, thus resolving the contradiction between adhesion strength and adaptability.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The amorphous solid electrolyte with alkali metal oxide and silicon oxide composition ensures excellent adhesion and densification without high-temperature firing, resulting in improved battery performance with high charge and discharge capacities and efficiencies.

Implementation Method 1

the solid electrolyte has excellent adhesion to the electrode

Methodology Applied
Scientific EffectAdhesion: Adhesive

Implementation Method 2

densifiable without being fired at high temperatures

Methodology Applied
Scientific EffectDensification:

Data Source

PatentEP4636887A1Solid electrolyte for secondary battery, electrode for secondary battery, all-solid-state secondary battery, and method for manufacturing all-solid-state secondary battery
Publication Date: 2025.10.22 NIPPON ELECTRIC GLASS CO LTD
  • EP4636887A1 patent drawingFigure 1~2
  • EP4636887A1 patent drawingFigure 3~4
  • EP4636887A1 patent drawing

AI summary

Provided is a solid electrolyte having excellent adhesion to the electrode and densifiable without being fired at high temperatures and, thus, capable of delivering good battery characteristics. A solid electrolyte for a sodium-ion secondary battery contains an alkali metal oxide and silicon oxide and is amorphous.