Automated Analyzer Probe Clogging Detection

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Solution Overview

Problem

Automatic analyzers face challenges in maintaining dispensing accuracy when dealing with high viscosity samples, as existing methods for detecting clogging using pressure sensors are unreliable and can lead to sample scattering and reduced processing capabilities.

Innovation Solution

Implementing a system that examines the sample probe for clogging before suction and performs cleaning operations to ensure the probe is clear, allowing for continuous stable dispensing by checking the state inside the probe every cycle and performing necessary cleaning operations.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If pressure sensor-based clogging detection is used during suction, then clogging can be detected, but the detection is unreliable for high viscosity samples and may lead to false positives

Engineering Contradiction:
Improveclogging detection reliabilityVSAvoidclogging detection accuracy
Core Design Contradiction:
ReliabilityVSMeasurement precision

Solution Approach 1:

The system performs clogging detection by examining pressure waveform characteristics (negative pressure peak value and residual pressure) after suction completion, rather than during suction. This preliminary examination approach allows accurate detection of high viscosity samples without interfering with the suction process itself, resolving the contradiction between detection reliability and measurement precision.

Inventive Principle:
Principle #10Preliminary action

2Reliability

If continuous monitoring and cleaning operations are performed, then dispensing accuracy is maintained, but processing time increases

Engineering Contradiction:
Improvedispensing accuracyVSAvoidprocessing speed
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The system performs clogging examination after each suction operation and automatically executes cleaning operations when clogging is detected, ensuring continuous reliable dispensing without manual intervention. This continuous automated monitoring and cleaning maintains high dispensing accuracy while minimizing processing time losses.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The system autonomously detects clogging through pressure waveform analysis and performs cleaning operations without operator intervention. This self-service capability maintains dispensing accuracy while optimizing processing speed by eliminating manual cleaning steps and false positive interruptions.

Inventive Principle:
Principle #25Self-service

3Ease of operation

If threshold-based clogging detection is used, then simple determination is achieved, but false detection occurs with high viscosity samples

Engineering Contradiction:
Improvedetermination simplicityVSAvoiddetection accuracy
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The system evaluates multiple pressure waveform parameters (negative pressure peak value and residual pressure) rather than relying on a single threshold. By analyzing the combination and relationship of these parameters, the system maintains simple automated determination while significantly improving detection accuracy for high viscosity samples, avoiding false positives.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach ensures that clogging is prevented or removed before suction, maintaining dispensing accuracy and reliability, even with high viscosity samples, by continuously checking and cleaning the sample probe.

Implementation Method 1

detect the clogging of the sample probe based on pressure variations by disposing a pressure sensor inside a dispensing flow route including the sample probe

Methodology Applied
Scientific EffectPressure sensor detection:

Implementation Method 2

the dispensing syringe is driven by a predetermined amount. In this manner, a predetermined amount of the sample is suctioned

Methodology Applied
Scientific EffectNegative pressure suction: Pressure Gradient

Data Source

PatentEP2878955B1Automated analyzer
Publication Date: 2018.09.05 HITACHI HIGH TECH CORP
  • EP2878955B1 patent drawingFigure 1
  • EP2878955B1 patent drawingFigure 2
  • EP2878955B1 patent drawingFigure 3

AI summary

To provide an automatic analyzer which is not influenced by fluidity or viscosity of a sample, and which can stably dispense the sample with dispensing accuracy by determining whether a flow route including a sample probe is in a stable and suction-available state when the sample is suctioned. In suction of the sample, before the sample is suctioned, in the flow route including the sample probe, the automatic analyzer determines whether the sample is in a suction-available state or in a suction-unavailable state, and performs cleaning on the flow route when it is determined that the sample is not in the suction-available state. Since the state in the flow route including the sample probe is determined before the sample is suctioned, the automatic analyzer can repeatedly perform a dispensing operation having improved reliability, without being influenced by the fluidity or the viscosity.