Anionic Polyurethane Urea Textile Coating for Wet Adhesion

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Solution Overview

Problem

Existing methods for coating sheet-form textile materials with polyurethane dispersions face challenges in achieving high wet adhesion due to the use of hydrophilic structural units, which lead to swelling and reduced adhesion, and are often costly and environmentally unfriendly.

Innovation Solution

An aqueous dispersion of anionically modified polyurethane urea, composed of aromatic diisocyanate, polyether polyol, isocyanate-reactive compounds with ionogenic groups, and polyamine, is applied to the textile material, providing a high content of urethane and urea groups for excellent adhesion while being environmentally harmless and cost-effective.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If polyurethanes containing hydrophilic structural units are used in aqueous polyurethane dispersions, then the polyurethane becomes dispersible in water, but the hydrophilic structural units lead to swelling of the polyurethane in water and reduce adhesion

Engineering Contradiction:
Improvedispersibility in waterVSAvoidadhesion
Core Design Contradiction:
Adaptability or versatilityVSStrength

Solution Approach 1:

The patent extracts the harmful effect of hydrophilic structural units by using anionic modification through reaction with isocyanate groups and compounds containing ionogenic groups (such as carboxylic acids, sulfonic acids, or their salts). This creates water dispersibility through ionic groups attached to the polyurethane backbone rather than through traditional hydrophilic structural units, thereby avoiding swelling while maintaining adhesion.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent changes the chemical parameter of the polyurethane by introducing anionic groups through modification reactions. The anionic groups (carboxylate, sulfonate, etc.) provide water dispersibility without causing swelling, thus resolving the contradiction between dispersibility and adhesion strength.

Inventive Principle:
Principle #35Parameter changes

2Strength

If polyurethanes are used as adhesive coat without hydrophilic structural units, then adhesion is maintained, but the use of organic solvents becomes necessary which is undesirable for economic and ecological reasons

Engineering Contradiction:
ImproveadhesionVSAvoidorganic solvent emission
Core Design Contradiction:
StrengthVSObject-generated harmful factors

Solution Approach 1:

The patent changes the chemical composition parameter by introducing anionic groups that enable water dispersibility. This allows the use of aqueous dispersions instead of organic solvent solutions, eliminating harmful solvent emissions while maintaining the adhesion properties needed for the adhesive coat.

Inventive Principle:
Principle #35Parameter changes

3Strength

If silylated polyurethanes are used to improve wet adhesion, then self-crosslinking components compensate for swellability, but the components are cost-intensive and release VOCs which is ecologically undesirable

Engineering Contradiction:
Improvewet adhesionVSAvoidcost and VOC emission
Core Design Contradiction:
StrengthVSObject-generated harmful factors

Solution Approach 1:

The patent extracts the problematic silyl groups and replaces them with anionic groups (carboxylate, sulfonate, etc.) that provide similar water dispersibility without requiring costly silylation steps or releasing VOCs. The anionic modification achieves the same goal of enabling aqueous dispersion without the harmful side effects.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent uses conventional, cost-effective anionic groups (from common acids like carboxylic or sulfonic acids) instead of expensive silylating agents. These anionic groups provide the necessary water dispersibility without requiring additional costly processing steps or releasing harmful VOCs.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method achieves excellent wet adhesion and high strength in coated textile materials, suitable for various textile forms, including woven and nonwoven fabrics, with a flexible and non-tacky adhesive coat that is inexpensive to produce and environmentally friendly.

Implementation Method 1

aqueous dispersion of anionically modified polyurethane urea

Methodology Applied
Scientific EffectDispersion: Dispersion (of waves)

Implementation Method 2

excellent wet adhesion and high strength in coated textile materials

Methodology Applied
Scientific EffectAdhesion: Adhesive

Data Source

PatentUS7972982B2Aqueous dispersion of anionically modified polyurethane ureas for coating a sheet-form textile material
Publication Date: 2011.07.05 COVESTRO DEUTSCHLAND AG

AI summary

The invention relates to a method for coating sheet-form textile materials, in which there is applied to a sheet-form textile material an aqueous dispersion containing anionically modified polyurethane ureas comprising (A) aromatic diisocyanate, (B) polyether polyol having a mean molecular weight greater than 1500, (C) at least one compound containing from 1 to 2 isocyanate-reactive groups and at least one ionogenic group, (D) polyamine having a mean molecular weight of at least 32, and (E) water, wherein the mean total functionality of the isocyanate-reactive compounds B to D is from 1.85 to 2.2, the molar ratio of the isocyanate groups of component A to the isocyanate-reactive groups of components B to D is greater than 1, and the polyurethane ureas have a content of from 800 to 1500 mmol of urethane groups/kg of anionically modified polyurethane urea and a content of from 800 to 1800 mmol of urethane plus urea groups/kg of anionically modified polyurethane urea.