Annular divided wall column with ring shaped collectors and distributers

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Solution Overview

Problem

Existing annular divided wall column systems for cryogenic rectification face challenges such as maldistribution of vapor and liquids, lower performance due to thermal expansion/contraction differences, and inadequate pressure boundaries, leading to increased capital costs and space requirements.

Innovation Solution

The design incorporates a first and second annular column wall with a plurality of structured packing elements, ring-shaped cantilevered collectors, and ring-shaped distributors, where the second annular column wall's thermal expansion and contraction are independent of the first, and the use of support structures like pivoting arms and rolled angle rings to reduce structural complexity and enhance performance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If divided-wall columns are used to reduce column cost and space requirements, then capital cost and space are reduced, but maldistribution of vapor and liquids occurs and performance deteriorates

Engineering Contradiction:
Improvecolumn costVSAvoidrectification performance
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The column is divided into multiple independent distillation sections (annulus column region and interior core column region) separated by an inner annular wall, allowing each section to function independently while sharing the same column shell, thereby reducing overall capital cost and space requirements while maintaining separation efficiency

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

An intermediate fluid barrier wall is positioned between the annulus column region and interior core column region to prevent direct mixing of vapor and liquid streams while allowing thermal interaction, thereby maintaining proper phase distribution and preventing maldistribution issues

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of manufacture

If divided-wall columns are used to reduce column cost and space requirements, then capital cost and space are reduced, but maldistribution of down-flowing liquids occurs due to large wall surface areas

Engineering Contradiction:
Improvecolumn costVSAvoidliquid distribution
Core Design Contradiction:
Ease of manufactureVSEase of operation

Solution Approach 1:

The fluid barrier wall is extracted from direct contact with liquid streams and repositioned as an intermediate thermal barrier, eliminating its negative impact on liquid distribution while preserving its thermal function, thereby improving liquid flow distribution in the annulus region

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

Different regions of the column are designed with different structural characteristics - the annulus column region has optimized wall surface area and liquid distribution structures tailored to its specific flow patterns, while the interior core column region has its own optimized configuration, allowing each region to operate at optimal performance

Inventive Principle:
Principle #3Local quality

3Productivity

If divided-wall columns are used with structured packing, then mass transfer efficiency is improved, but transient thermal expansion/contraction differences between inner and outer shells cause performance degradation

Engineering Contradiction:
Improvemass transfer efficiencyVSAvoidperformance stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The column design accommodates dynamic thermal expansion and contraction by allowing the inner annular wall and fluid barrier wall to move independently relative to the outer shell, preventing stress buildup and maintaining structural integrity and performance stability during transient thermal conditions

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The intermediate fluid barrier wall acts as a thermal buffer between the inner and outer shells, absorbing and distributing thermal stresses to reduce the impact of thermal expansion differences on the structured packing and overall column performance

Inventive Principle:
Principle #24Intermediary (Mediator)

4Area of stationary object

If divided-wall columns are used to reduce space requirements, then column footprint is reduced, but the pressure boundary between interior core and annulus regions becomes inadequate

Engineering Contradiction:
Improvecolumn footprintVSAvoidpressure boundary
Core Design Contradiction:
Area of stationary objectVSStress or pressure

Solution Approach 1:

The pressure boundary functions are merged into the common outer column shell, which is designed to withstand the combined pressure loads from both the annulus column region and interior core column region, thereby providing adequate pressure containment while maintaining a compact footprint

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration improves vapor and liquid distribution, enhances performance by allowing independent thermal expansion, and reduces capital costs and space requirements, resulting in a more efficient and cost-effective cryogenic rectification system.

Implementation Method 1

a plurality of packing elements or trays disposed within the interior core column region and the annulus column region

Methodology Applied
Scientific EffectMass transfer: Diffusion

Implementation Method 2

one or more ring-shaped distributors disposed in the annulus column region above or below the plurality of structured packing elements

Methodology Applied
Scientific EffectFluid distribution:

Implementation Method 3

one or more ring-shaped cantilevered collectors disposed in the annulus column region above or below the plurality of structured packing elements

Methodology Applied
Scientific EffectVapor flow management:

Implementation Method 4

wherein thermal expansion and contraction of the second annular column wall in a radial direction and in an axial direction is independent of the thermal expansion and contraction of the first annular column wall in radial and axial directions

Methodology Applied
Scientific EffectThermal expansion: Thermal Expansion

Data Source

PatentUS10866025B2Annular divided wall column with ring shaped collectors and distributers
Publication Date: 2020.12.15 PRAXAIR TECH INC
  • US10866025B2 patent drawing
  • US10866025B2 patent drawing
  • US10866025B2 patent drawing

AI summary

An annular divided wall column for the cryogenic rectification of air or constituents of air is provided. The annular divided wall column includes a first annular column wall and a second annular column wall disposed within the first annular column wall to define an annulus column region and an interior core column region. The present annular divided wall column further includes structured packing elements disposed within at least the annulus column region as well as a ring-shaped cantilevered collector; and a ring-shaped distributor disposed in the annulus column region above or below the plurality of structured packing elements. The thermal expansion and contraction of the second annular column wall in a radial direction and in an axial direction is independent of the thermal expansion and contraction of the first annular column wall in the radial and axial directions.