Anodic Oxidation Mold for Antireflection Without Joint Lines

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Solution Overview

Problem

Producing large area molds or roll molds with microscopic patterns smaller than the wavelength of visible light is challenging due to issues like joint line remnants, low yield, and high production costs, as well as macroscopic unevenness from existing methods.

Innovation Solution

A process involving anodic oxidation of aluminum to create a mold with a regular microscopic pattern without joint lines or visible unevenness, using a combination of first and second anodic oxidation steps and pore diameter enlargement to achieve a smooth, tapered pore structure suitable for antireflection applications.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a large area mold or roll mold with microscopic pattern is produced by conventional lithography or assembly methods, then the mold can be used for mass production, but joint lines remain visible and yield is low

Engineering Contradiction:
Improvemass production capabilityVSAvoidyield
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The invention divides the mold production process into two independent stages: (1) producing a master mold with microscopic pattern by lithography on a small substrate, and (2) replicating this pattern onto a large area mold or roll mold through contact copying. This segmentation allows the master mold to be small and free of joint lines, while the replicated large mold inherits the pattern without introducing joint line defects.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention uses a contact copying process where a master mold with the microscopic pattern is pressed against a larger substrate to transfer the pattern. This copying method eliminates the need to directly fabricate the large mold with lithography, thereby avoiding joint line issues and improving yield through simpler, more reliable pattern transfer.

Inventive Principle:
Principle #26Copying

2Manufacturing precision

If lithography is used to form microscopic pattern not larger than visible light wavelength over large area, then the pattern resolution is sufficient, but the process complexity and production cost increase significantly

Engineering Contradiction:
Improvepattern resolutionVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The invention separates the high-precision pattern formation step from the large area coverage step. The master mold is fabricated with the required sub-wavelength precision using lithography on a small, manageable substrate. Subsequently, this precise pattern is replicated onto large substrates through simple contact copying, which does not require lithographic precision but achieves large area coverage efficiently.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The contact copying process transfers the high-resolution pattern from the master mold to large area substrates without requiring the copying process itself to have lithographic precision. This dramatically simplifies the overall process complexity and reduces production costs while maintaining the required pattern resolution.

Inventive Principle:
Principle #26Copying

3Ease of manufacture

If anodic oxidation is used to create microscopic pattern on aluminum, then the process is simple and economical, but macroscopic unevenness from rolling marks or crystal grain boundaries becomes visible

Engineering Contradiction:
Improveprocess simplicityVSAvoidsurface uniformity
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The invention performs preliminary surface treatment of the aluminum substrate before anodic oxidation to eliminate macroscopic unevenness. The substrate undergoes mechanical polishing, chemical polishing, or electropolishing to remove rolling marks and level crystal grain boundaries. This preliminary action ensures that the subsequent anodic oxidation produces a uniform microscopic pattern without visible macroscopic defects.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method allows for the simple and economical production of molds and sheets with microscopic patterns, ensuring high yield and optical quality by eliminating joint lines and macroscopic unevenness, thereby enhancing antireflection properties.

Implementation Method 1

anodic oxidation of aluminum to create a mold with a regular microscopic pattern

Methodology Applied
Scientific EffectAnodic oxidation: Anodising

Implementation Method 2

a steric structure called as a moth-eye structure is known as an effective antireflection means due to gradual increase from a refractive index of air to a refractive index of a material

Methodology Applied
Scientific EffectMoth-eye structure antireflection: Anti-Reflective Coating

Data Source

PatentEP2045368B8Mold, process for manufacturing mold, and process for producing sheet
Publication Date: 2016.12.07 MITSUBISHI RAYON CO LTD

AI summary

A mold comprising alumina having a microscopic pattern, in which distances between adjacent recesses or salients therein are not longer than wavelength of visible light, formed by anodic oxidation on a surface of an alminum pre-mold without a rolling mark, wherein height or depth difference at a crystal grain boundary is 300 nm or less.