Antifouling Silane Composition for Hardness and Water Repellency

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing antifouling coatings face issues with surface hardness, friction properties, and environmental concerns, as well as vulnerability to scratches and stains, which affect their water repellency and durability.

Innovation Solution

A composition comprising a tetrafunctional silane-based compound, trifunctional silane-based compounds, and a metal catalyst, specifically formulated to enhance surface hardness, friction properties, and water repellency, while being environmentally friendly.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a fluorine-containing compound is used to form a water-repellent film, then water repellency is improved, but environmental protection is worsened

Engineering Contradiction:
Improvewater repellencyVSAvoidenvironmental protection
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The invention changes the chemical composition parameters by replacing fluorine-containing compounds with silicon-based compounds having specific molecular structures (formulae 1 and 2 with defined R1-R6 groups). This substitution maintains water repellency through hydrophobic alkyl groups while eliminating environmental harm associated with fluorine compounds.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses composite silane-based materials combining multiple functional groups (alkoxy groups for crosslinking, alkyl groups for hydrophobicity) within a single molecular structure. This composite approach achieves both water repellency and environmental compatibility without relying on harmful fluorine compounds.

Inventive Principle:
Principle #40Composite materials

2Strength

If the antifouling layer is made softer to reduce scratches, then surface hardness is reduced, but water slipping properties are worsened

Engineering Contradiction:
Improvesurface hardnessVSAvoidwater slipping properties
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The invention optimizes the molecular structure parameters of the silane-based compounds, specifically the length and branching of alkyl groups (R1-R6) and the ratio of alkoxy to alkyl groups. This parameter optimization achieves a balance where the crosslinked network provides hardness while the hydrophobic alkyl chains maintain water slipping properties.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The antifouling layer uses a composite molecular structure combining a crosslinked silicon oxide network (for hardness) with long hydrophobic alkyl side chains (for water slipping). This composite structure at the molecular level simultaneously achieves both surface hardness and water repellency without compromise.

Inventive Principle:
Principle #40Composite materials

3Strength

If the antifouling layer is made harder to improve scratch resistance, then surface hardness is improved, but friction properties are worsened

Engineering Contradiction:
Improvesurface hardnessVSAvoidfriction properties
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The invention carefully controls the molecular parameters including the carbon number of alkyl groups (6-20 carbons) and the molar ratio of different silane components. These parameter adjustments ensure the surface is hard enough for scratch resistance but maintains low friction through the hydrophobic molecular structure that prevents water and stain adhesion.

Inventive Principle:
Principle #35Parameter changes

4Ease of manufacture

If a simple silane composition is used to reduce complexity, then manufacturing complexity is reduced, but surface state and curability are worsened

Engineering Contradiction:
Improvemanufacturing complexityVSAvoidsurface state and curability
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The invention segments the silane-based compound into multiple functional components within the molecular structure: alkoxy groups for controlled crosslinking, alkyl groups for hydrophobicity, and specific structural units for surface morphology control. This segmentation allows each component to perform its function independently, achieving excellent surface state and curability.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention employs composite silane chemistry combining tetrafunctional silanes (for crosslinking density) with trifunctional silanes (for surface properties). This composite material approach at the molecular level achieves superior curability and surface state while maintaining relatively simple manufacturing processes.

Inventive Principle:
Principle #40Composite materials

5Reliability

If the antifouling layer is made more resistant to stains, then stain resistance is improved, but surface hardness may be compromised

Engineering Contradiction:
Improvestain resistanceVSAvoidsurface hardness
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The invention adjusts the hydrophobicity parameters by selecting alkyl groups with specific carbon numbers (6-20) and controlling their density on the molecular structure. This parameter optimization creates a surface that is highly resistant to stain adhesion through hydrophobic effects while the crosslinked silicon network maintains adequate surface hardness.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides an antifouling layer with improved surface hardness, low friction, and excellent water repellency, ensuring effective water slipping and resistance to stains and scratches, while being environmentally sustainable.

Implementation Method 1

a tetrafunctional silane-based compound represented by general formula (a)... a trifunctional silane-based compound represented by general formula (b)... a trifunctional silane-based compound represented by general formula (c)... and a metal catalyst

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 2

a tetrafunctional silane-based compound... at least two trifunctional silane-based compounds... and a metal catalyst

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

a tetrafunctional silane-based compound... at least two trifunctional silane-based compounds... and a metal catalyst

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 4

the surfaces are given water repellency or antifouling properties... favorable water repellency and water slipping properties

Methodology Applied
Scientific EffectHydrophobe: Hydrophobe

Data Source

PatentEP3323865B1Antifouling composition, antifouling sheet, and process for producing antifouling sheet
Publication Date: 2020.09.02 LINTEC CORP
  • EP3323865B1 patent drawingFigure 1(a)~2(b)

AI summary

Provided are an antifouling composition including a tetrafunctional silane-based compound having a specified structure as a component (A), trifunctional silane-based compounds having a specified structure different from each other as a component (B) and component (C), and a metal catalyst as a component (D), the antifouling composition satisfying: Condition (I): a ratio of a molar amount of the component (A) to a molar amount of the component (B) [(A)/(B)] (molar ratio) is 1.4 or more, and Condition (II): a ratio of a molar amount of the component (B) to a total molar amount of the component (B) and the component (C) [(B)/{(B) + (C)}] (molar ratio) is 0.020 or more, an antifouling sheet including an antifouling layer formed of the antifouling composition, and a method for producing the same.