Aqueous Electrolyte Metal Cation Anode Protection

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Solution Overview

Problem

Aqueous lithium ion secondary batteries using high-concentration aqueous electrolyte solutions face challenges with electrolysis on the anode surface due to overvoltage, leading to unstable charge/discharge cycles.

Innovation Solution

An aqueous electrolyte solution comprising water, a lithium ion, at least one imide-based anion (TFSI or FSI), and a metal cation, with specific concentrations and pH levels, is used to suppress electrolysis by electrodeposition of metal cations with low work functions on the anode surface, reducing direct contact between the electrolyte and high-work-function areas.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If high-concentration aqueous electrolyte solution is used, then potential window range is expanded, but electrolysis occurs on anode surface due to overvoltage

Engineering Contradiction:
Improvepotential window rangeVSAvoidcharge/discharge cycle stability
Core Design Contradiction:
Adaptability or versatilityVSReliability

Solution Approach 1:

The patent changes the chemical composition parameters of the electrolyte by introducing specific metal cations (Mg2+, Ca2+, Sr2+, Ba2+) at controlled concentrations (0.001-0.1 mol/kg) into the high-concentration aqueous electrolyte. This parameter modification suppresses electrolysis on the anode surface while preserving the expanded potential window, thereby resolving the contradiction between adaptability and reliability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The metal cations act as intermediary substances that mediate between the high-concentration electrolyte and the anode surface. These cations preferentially adsorb on the anode surface, forming a protective layer that prevents direct contact between the electrolyte and anode, thus suppressing electrolysis reactions while allowing the high-concentration electrolyte to maintain its expanded potential window

Inventive Principle:
Principle #24Intermediary (Mediator)

2Quantity of substance

If high-concentration aqueous electrolyte solution is used, then energy density per volume is improved, but charge/discharge cycles become unstable

Engineering Contradiction:
Improveenergy density per volumeVSAvoidcharge/discharge cycle stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent modifies the electrolyte composition by adding specific metal cations at optimized concentrations to the high-concentration aqueous electrolyte. This parameter change suppresses electrolysis side reactions that degrade cycle stability, allowing the battery to maintain both high energy density and stable charge/discharge cycles

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The metal cations serve as intermediary substances that stabilize the interface between the electrolyte and anode. By preferentially adsorbing on the anode surface, they prevent direct electrolysis of the high-concentration electrolyte, thereby preserving both the high energy density and cycle stability

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach stabilizes charge/discharge cycles and improves the cycle characteristics of aqueous lithium ion secondary batteries by reducing electrolysis on the anode surface, enhancing the battery's performance and longevity.

Implementation Method 1

electrodeposition of metal cations with low work functions on the anode surface

Methodology Applied
Scientific EffectElectrodeposition: Electrodeposition

Implementation Method 2

there is a case where an aqueous electrolyte solution is electrolyzed on a surface of an anode due to overvoltage etc.

Methodology Applied
Scientific EffectElectrolysis: Electrolysis

Data Source

PatentEP3509158B1Aqueous electrolyte solution, and aqueous lithium ion secondary battery
Publication Date: 2023.07.05 TOYOTA JIDOSHA KK
  • EP3509158B1 patent drawingFigure 1
  • EP3509158B1 patent drawingFigure 2A~2F
  • EP3509158B1 patent drawingFigure 3A~3D

AI summary

Electrolysis of an aqueous electrolyte solution on a surface of an anode is suppressed when an aqueous lithium ion secondary battery is charged/discharged. In an aqueous electrolyte solution that is used for an aqueous lithium ion secondary battery, at least one metal cation selected from an aluminum ion, a titanium ion, a manganese ion, a zinc ion, a gallium ion, a yttrium ion, a zirconium ion, an indium ion, a lanthanum ion, a cerium ion, a neodymium ion, and a hafnium ion is contained so that its content is more than 0 mol and no more than 0.01 mol per kilogram of the aqueous electrolyte solution, in addition to a lithium ion and at least one imide based anion.