Aqueous Primer Composition with Reactive Epoxy Coalescence

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Solution Overview

Problem

Existing aqueous primer compositions for aircraft structures face issues with stability during storage and application, poor wetting capability, and reduced chemical and corrosion resistance due to the unique wetting behavior of aqueous compositions, leading to rough and powdery coatings that are prone to chips and scratches.

Innovation Solution

Aqueous primer compositions using a reactive liquid epoxy as a coalescent agent, allowing for the formation of a continuous film without the need for organic solvents, by coalescing resin particles during drying and curing, with a curative that is water-insoluble and reactive with the resins.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If organic solvent is introduced into the emulsion to coalesce resin particles, then film-forming ability is improved, but storage stability is reduced and wetting capability deteriorates

Engineering Contradiction:
Improvefilm-forming abilityVSAvoidstorage stability
Core Design Contradiction:
Manufacturing precisionVSStability of the object's composition

Solution Approach 1:

The patent changes the chemical nature of the coalescent from traditional organic solvents to a reactive liquid epoxy resin. This parameter change allows the coalescent to remain effective at lower concentrations while improving storage stability and maintaining wetting capability through its reactive chemistry and controlled film formation mechanism.

Inventive Principle:
Principle #35Parameter changes

2Object-affected harmful factors

If aqueous composition is used as primer, then volatile organic solvent emissions are reduced, but coating uniformity and surface quality deteriorate

Engineering Contradiction:
Improvevolatile organic solvent emissionsVSAvoidcoating uniformity
Core Design Contradiction:
Object-affected harmful factorsVSManufacturing precision

Solution Approach 1:

The patent creates a composite aqueous primer system combining water-based emulsion with reactive liquid epoxy resin as coalescent. This composite approach maintains the environmental benefits of aqueous formulations while achieving uniform coating quality through the synergistic interaction between the emulsion particles and the reactive coalescent that forms a continuous film during curing.

Inventive Principle:
Principle #40Composite materials

3Reliability

If high melting point thermosetting resin is used in aqueous dispersion, then corrosion resistance is improved, but film smoothness and continuity deteriorate

Engineering Contradiction:
Improvecorrosion resistanceVSAvoidfilm smoothness
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The reactive liquid epoxy resin acts as an intermediary between the high melting point thermosetting resin particles and the aqueous medium. During drying and curing, this intermediary facilitates the coalescence of rigid particles into a smooth, continuous film while maintaining the corrosion-resistant properties of the thermosetting resin network.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides a uniform, continuous primer film with improved surface protection and high storage stability, enhancing handling and corrosion resistance.

Implementation Method 1

a second thermosetting resin that is liquid at ambient conditions and acting as a reactive coalescent agent in which the first thermosetting resin is at least partially soluble

Methodology Applied
Scientific EffectDissolution: Solvation

Implementation Method 2

Aqueous primers, which use water as a volatile solvent, are provided in the form of a latex-emulsified particles of a thermosetting resin dispersed in aqueous dispersion. Typically, the dispersion is coated onto a substrate, dried, and then heated to cure the thermosetting resin.

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS12448525B2Aqueous primer compositions and methods thereof
Publication Date: 2025.10.21 3M INNOVATIVE PROPERTIES CO

AI summary

Provided is an aqueous primer composition including a first thermosetting resin that is a particulate solid at ambient conditions and a second thermosetting resin that is liquid at ambient conditions and acting as a reactive coalescent agent in which the first thermosetting resin is at least partially soluble. The second thermosetting resin acts as a coalescent agent to enable a continuous primer film to be formed as the primer is being dried before it is cured. The composition further includes a curative that is substantially water-insoluble and reactive with the first and second thermosetting resins. The overall composition can contain up to 4 percent by weight of volatile solvents, other than water and provides a shelf-stable primer that can form a continuous film without the need for added organic solvents.