Area Selective Atomic Layer Deposition via Segmented Gas Zones

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Solution Overview

Problem

Existing atomic layer deposition (ALD) methods lack spatial control and high throughput for area-selective deposition, leading to inefficiencies in gas usage and process steps, particularly in large-scale or high-throughput applications.

Innovation Solution

An atomic layer deposition device with a process gas injection head and conveying system that provides relative movement between the substrate and gas injection head, utilizing multiple deposition and separator spaces to selectively apply precursor and co-reactant gases while minimizing gas intermixing, using a combined separator-inhibitor gas flow to prevent deposition on non-target areas.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional vacuum-based ALD methods are used for area-selective deposition, then deposition selectivity can be achieved, but long evacuation steps are required and gas usage increases

Engineering Contradiction:
Improvedeposition selectivityVSAvoidevacuation step duration
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The reaction chamber is divided into multiple independently controllable zones (first reaction zone, second reaction zone, third reaction zone) with separate gas injection and evacuation systems. This segmentation allows selective evacuation of specific zones containing unwanted reactions, eliminating the need to evacuate the entire chamber and reducing overall evacuation time while maintaining deposition selectivity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different zones of the reaction chamber are assigned different functions: the first zone handles precursor delivery, the second zone performs the actual deposition reaction, and the third zone manages inhibitor gas delivery and evacuation. Each zone has optimized gas flow rates and pressures tailored to its specific function, improving overall efficiency and reducing unnecessary evacuation steps.

Inventive Principle:
Principle #3Local quality

2Manufacturing precision

If conventional ALD methods are used, then deposition control is maintained, but gas usage increases due to multiple evacuation steps

Engineering Contradiction:
Improvedeposition controlVSAvoidgas usage
Core Design Contradiction:
Manufacturing precisionVSLoss of substance

Solution Approach 1:

The chamber is segmented into multiple zones with independent gas management systems. This allows selective gas delivery to specific zones and localized evacuation, preventing gas from being wasted throughout the entire chamber. Gas is only evacuated from zones where reactions occur, significantly reducing overall gas consumption while maintaining precise deposition control.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system dynamically adjusts gas flow rates, pressures, and temperatures in different zones based on the specific deposition requirements. By optimizing these parameters locally in each zone, the system achieves precise deposition control while minimizing gas usage through more efficient gas utilization in each regional area.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If high-throughput deposition is implemented, then productivity increases, but spatial control over deposition areas is lost

Engineering Contradiction:
Improvedeposition throughputVSAvoidspatial control
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The reaction chamber is divided into multiple spatially separated zones with independent gas injection heads and evacuation systems. This segmentation enables simultaneous operations in different zones: while one zone performs deposition, another handles precursor delivery or inhibitor gas delivery. The system maintains spatial control by physically separating reaction zones and controlling gas flow to specific areas, achieving high throughput without sacrificing precision.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system adds a temporal dimension to the deposition process by performing multiple deposition cycles simultaneously in different spatial zones. While one zone completes a full deposition cycle, another zone prepares the next cycle, creating overlapping operations that increase throughput. This multi-dimensional approach (space-time separation) maintains spatial control through physical zone separation while achieving high productivity through parallel processing.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables efficient, high-throughput, and area-selective deposition of target material layers by reducing gas usage and eliminating the need for long evacuation steps, while maintaining precise control over deposition areas.

Implementation Method 1

a conveying system arranged to provide relative movement, including but not limited to linear reciprocation and rotation, between the substrate surface and the process gas injection head in a direction along the substrate surface to form a conveying plane

Methodology Applied
Scientific EffectMechanical movement:

Implementation Method 2

inhibitor moieties selectively adhering to the non-deposition area

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 3

the precursor gas flow for adsorbing precursor moieties to the pre-defined deposition area of the substrate surface

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 4

the co-reactant gas flow to allow co-reactant moieties comprised therein to react with adsorbed precursor moieties to form a first layer of target material

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentEP4058617B1Area selective atomic layer deposition method and tool
Publication Date: 2023.09.27 NEDERLANDSE ORG VOOR TOEGEPAST NATUURWETENSCHAPPELIJK ONDERZOEK TNO
  • EP4058617B1 patent drawingFigure 1A~1B
  • EP4058617B1 patent drawingFigure 2
  • EP4058617B1 patent drawingFigure 3

AI summary

The present disclosure concerns an atomic layer deposition device for area-selective deposition of a target material layer onto a deposition area of a substrate surface further comprising a non- deposition area. In use the substrate is conveyed along a plurality of deposition and separator spaces including at least two gas separator spaces provided with at least a separator gas inlet and a separator drain for, in use exposing the substrate to a separator gas flow. Wherein at least one of the gas separator spaces forms a combined separator-inhibitor gas flow comprising a separator gas and inhibitor moieties. The inhibitor moieties selectively adhering to the non-deposition area to form an inhibition layer reducing adsorption of precursor moieties. In a preferred embodiment the device includes a back-etching space to increase selectivity of the deposition process.