Argon Column Intermediate Storage for Rapid Load Rate Adjustment

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Solution Overview

Problem

Existing air separation units face challenges in maintaining constant L/V ratios during changes in argon column load rates, leading to inefficiencies and limitations in rate adjustments.

Innovation Solution

Installation of intermediate liquid storage capacities at the outlet of distributors to manage liquid reflux during load changes, allowing for quicker adjustments in argon production rates without additional equipment, utilizing a system of stacked storages and a condenser for efficient liquid management.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the argon column load rate is changed rapidly, then the productivity increases, but the L/V ratio becomes unstable and efficiency decreases

Engineering Contradiction:
Improveargon production rateVSAvoidL/V ratio
Core Design Contradiction:
ProductivityVSStability of the object's composition

Solution Approach 1:

The invention installs intermediate liquid storage capacities at the outlet of distributors that are filled with excess liquid during load decreases and used during load increases. This preliminary storage of liquid ensures that the column maintains adequate liquid levels and L/V ratios during rapid load changes, enabling productivity increases to 5%/min while maintaining separation efficiency.

Inventive Principle:
Principle #10Preliminary action

2Stability of the object's composition

If additional equipment is added to maintain L/V ratios during load changes, then the stability improves, but the device complexity increases

Engineering Contradiction:
ImproveL/V ratioVSAvoidequipment configuration
Core Design Contradiction:
Stability of the object's compositionVSDevice complexity

Solution Approach 1:

The invention integrates the liquid storage function directly into the existing column structure by installing intermediate storage capacities at the outlet of distributors. This merging of storage and separation functions within a single integrated structure maintains L/V ratio stability during load changes without requiring separate external storage systems or additional complex equipment.

Inventive Principle:
Principle #5Merging (Combining)

3Device complexity

If the column operates without intermediate storage capacities, then the device complexity is reduced, but the liquid supply becomes insufficient during load increases

Engineering Contradiction:
Improvecolumn structureVSAvoidliquid reflux
Core Design Contradiction:
Device complexityVSQuantity of substance

Solution Approach 1:

The intermediate storage capacities are pre-filled with excess liquid during periods of reduced load or normal operation. When load increases occur, this pre-stored liquid is immediately available to maintain adequate liquid supply and reflux conditions, preventing liquid deficiency without requiring complex real-time liquid addition systems.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables rapid modifications in argon production rates, reaching up to 5%/min or more, while maintaining operational efficiencies by ensuring consistent liquid supply and reflux management.

Implementation Method 1

the liquid vaporized in the overhead condenser being returned to the column system

Methodology Applied
Scientific EffectVaporization: Evaporation

Implementation Method 2

producing argon by cryogenic distillation of an air gas

Methodology Applied
Scientific EffectCryogenic distillation: Distillation

Implementation Method 3

cryogenic distillation of air

Methodology Applied
Scientific EffectCryogenics: Cryogenics

Data Source

PatentEP3604994B1Method and device for producing argon by cryogenic distillation of air
Publication Date: 2021.01.13 LAIR LIQUIDE SA POUR LETUDE & LEXPLOITATION DES PROCEDES GEORGES CLAUDE
  • EP3604994B1 patent drawingFigure 1

AI summary

Argon production apparatus by cryogenic distillation comprising an argon separation column (K), means for sending a gas containing argon and oxygen (ORG) to the column, means for extracting an argon-enriched fluid (ARG) from the top of the column, means for extracting an oxygen-enriched liquid (ORL) from the column tank and at least two storages (S1, S2, S3, S4, S5, S6), arranged one above the other, each storage being connected to two different intermediate levels of the argon separation column by two pipes, the two storages being contiguous.