ASA Surface Sizing Composition Reducing Equipment Fouling

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Solution Overview

Problem

The use of alkenylsuccinic anhydride (ASA) as a surface sizing agent in paper production leads to significant fouling or deposit formation on paper-making equipment, particularly when calcium ions are present, which affects the efficiency and environmental sustainability of the process.

Innovation Solution

A surface sizing composition is prepared by separately adding an aqueous dispersion of alkenylsuccinic anhydride and a non-ionic, amphoteric, cationic, or anionic polymer to an aqueous solution with high water content, including starch, to minimize deposit formation on application equipment.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If ASA is used as a surface sizing agent, then hydrophobic properties and sizing effectiveness are improved, but deposit formation on equipment increases significantly

Engineering Contradiction:
Improvesizing effectivenessVSAvoiddeposit formation
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

A cationic polymer is introduced as an intermediary substance between ASA and the equipment surface. The polymer adsorbs onto the equipment surface first, creating a protective layer that prevents ASA from directly depositing on the equipment. This mediator approach allows ASA to perform its sizing function while the polymer protects the equipment from fouling

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The application sequence is changed from simultaneous mixing to sequential addition. ASA is added first to the aqueous component, allowed to distribute, then the cationic polymer is added subsequently. This parameter change in addition sequence allows the polymer to modify the surface properties after ASA has been positioned, preventing deposit formation without compromising sizing effectiveness

Inventive Principle:
Principle #35Parameter changes

2Reliability

If internal sizing agents are used, then sizing is achieved during paper formation, but size retention is lower than 100% and agents are lost in white water

Engineering Contradiction:
Improvesizing during formationVSAvoidsize agent loss
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

ASA is applied to the paper web surface immediately after formation while the web is still wet. This preliminary action allows the sizing agent to be positioned on the formed web rather than being mixed into the pulp during formation, improving size retention and reducing loss to white water while still achieving effective sizing

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly reduces deposit formation on size press equipment, allowing for effective surface sizing of paper while maintaining the hydrophobic properties of ASA, thus optimizing the paper-making process and reducing environmental impact.

Implementation Method 1

it has been found that use of ASA as a surface sizing agent under practical paper-making-conditions involves an increased problem with fouling of the paper-making equipment

Methodology Applied
Scientific EffectHydrophobic property: Hydrophobe

Implementation Method 2

Alkenylsuccinic anhydride-based sizing agents belong to the group of cellulose-reactive sizing agent

Methodology Applied
Scientific EffectChemical reaction with cellulose: Chemical Bonding

Implementation Method 3

Aqueous dispersions of ASA have, per se, a strong tendency to form deposits on equipment surfaces, in particular on the surfaces of size press rollers

Methodology Applied
Scientific EffectDeposit formation reduction: Deposition (physical)

Data Source

PatentEP2593604B1Surface sizing of paper
Publication Date: 2014.05.14 CHEM FAB BRUHL MARE

AI summary

The invention relates to a process for the preparation of surface sizing composition comprising separately adding to an aqueous component comprising at least 80 wt% of water: (a) an aqueous dispersion comprising an alkenylsuccinic anhydride (ASA); and, (b) a non-ionic, amphoteric, cationic, or anionic polymer. The invention also relates to a composition obtainable thereby and a process for surface treatment of paper.