Asphalt Oxidation Recycle Loop Dynamics

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Solution Overview

Problem

Conventional air blowing techniques for oxidizing asphalt are mass transfer limited, making it difficult to achieve the required softening point and penetration values for roofing applications, especially with 'hard' asphalt fluxes that cannot be adequately processed using standard methods.

Innovation Solution

The method involves using a recycle loop in the air blowing process to distribute an oxygen-containing gas throughout the asphalt flux, increasing the surface area of oxygen bubbles and reducing processing time, which allows for more efficient oxidation and production of asphalt with desired properties for roofing applications.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If conventional air blowing techniques are used to oxidize asphalt flux, then the softening point increases, but the processing time becomes excessively long and mass transfer is limited

Engineering Contradiction:
Improvesoftening pointVSAvoidprocessing time
Core Design Contradiction:
TemperatureVSLoss of time

Solution Approach 1:

The patent introduces mechanical agitation to dynamically mix the asphalt flux during oxidation, transforming the static mass transfer process into a dynamic one. This agitation continuously redistributes the asphalt molecules and oxygen bubbles, preventing stagnant zones and significantly accelerating the oxidation reaction rate, thereby reducing processing time while achieving the required softening point

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent employs spargers to inject oxygen-containing gas into the asphalt flux in controlled bubbles, and uses mechanical agitation to disperse these bubbles throughout the material. This pneumatic-hydraulic system ensures uniform oxygen distribution and maximizes the gas-liquid interfacial area, dramatically improving mass transfer efficiency and reducing oxidation time

Inventive Principle:
Principle #29Pneumatics and hydraulics

2Manufacturing precision

If air blowing is performed for extended periods to achieve desired penetration values, then oxidation is complete, but energy consumption increases and yield decreases

Engineering Contradiction:
Improvepenetration valueVSAvoidenergy consumption
Core Design Contradiction:
Manufacturing precisionVSLoss of energy

Solution Approach 1:

By introducing mechanical agitation, the patent creates a dynamic mixing environment that uniformly distributes oxygen throughout the asphalt flux. This prevents localized over-oxidation and ensures consistent penetration values are achieved more quickly, reducing the extended processing times and associated energy consumption of conventional methods

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent optimizes oxidation parameters including oxygen injection rate, agitation speed, and temperature to achieve the desired penetration value efficiently. By carefully controlling these parameters, the process reaches the target penetration range without excessive energy input or prolonged processing that would reduce yield

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If conventional sparging methods are used to introduce oxygen, then the process is simple, but mass transfer is limited and oxidation efficiency is low

Engineering Contradiction:
Improveprocess simplicityVSAvoidoxidation efficiency
Core Design Contradiction:
Ease of manufactureVSProductivity

Solution Approach 1:

The patent adds mechanical agitation to the simple sparging process, creating a dynamic system where asphalt flux is continuously mixed and oxygen bubbles are uniformly distributed. This modest increase in complexity dramatically improves mass transfer and oxidation efficiency, achieving a favorable balance between process simplicity and productivity

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The combination of spargers for oxygen injection and mechanical agitation creates an efficient pneumatic-hydraulic system. The spargers provide controlled oxygen delivery while the agitation ensures thorough mixing and bubble dispersion, together achieving high oxidation efficiency with only moderate increases in process complexity

Inventive Principle:
Principle #29Pneumatics and hydraulics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach reduces the time and energy required for air blowing, increases yield, minimizes environmental impact, and achieves the necessary softening point and penetration values for roofing asphalt, enhancing productivity and cost-effectiveness.

Implementation Method 1

The air blowing process results in the stiffness and the softening point of the asphalt flux being significantly increased

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 2

a pump and air injection port are located on the recycle loop with the oxygen containing gas being added into the recycle loop just before the pump

Methodology Applied
Scientific EffectPumping: Pump

Implementation Method 3

The pump generates small bubbles of the oxygen containing gas within the asphalt flux in the blow still and accordingly increases the surface area of the bubbles

Methodology Applied
Scientific EffectBubble formation and dispersion: Bubble

Data Source

PatentUS9556383B2Asphalt oxidation technique
Publication Date: 2017.01.31 BMIC LLC
  • US9556383B2 patent drawing
  • US9556383B2 patent drawing

AI summary

The present invention relates to a method for oxidizing asphalt which comprises dispersing an oxygen containing gas throughout an asphalt flux in an oxidation zone while the asphalt flux is maintained at a temperature which is within the range of about 400° F. to 550° F., wherein the oxygen containing gas is introduced into the oxidation zone through a recycle loop. The recycle loop pumps asphalt flux from the oxidation zone and reintroduces the asphalt flux into the oxidation zone as oxygen enhanced asphalt flux. The recycle loop will typically include a pump which pulls the asphalt flux from the oxidation zone and which pumps the oxygen enhanced asphalt flux into the oxidation zone, and wherein the oxygen containing gas is injected into the recycle loop at a point before the asphalt flux enters into the pump.