Asphaltic Sheet Processing With Expandable Graphite Below Char Temperature

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Solution Overview

Problem

The use of intumescent materials as flame retardants in asphaltic sheets is limited by the need to maintain processing temperatures below the char-forming temperature, restricting their incorporation and expanding the scope of useful materials.

Innovation Solution

A method involving the preparation of a masterbatch with asphalt binder and polymeric modifier, followed by cooling and the addition of expandable graphite at a temperature below the char-forming point, allowing for the incorporation of intumescent materials without triggering their expansion, thereby enabling the production of asphaltic sheets with enhanced fire resistance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If intumescent materials are incorporated into asphaltic sheet at high processing temperatures, then flame resistance is improved, but the intumescent material undergoes premature char-forming expansion which frustrates manufacturing

Engineering Contradiction:
Improveflame resistanceVSAvoidmanufacturing feasibility
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent applies preliminary action by incorporating the intumescent material (expandable graphite) into the asphaltic composition before the final manufacturing step, but at a controlled lower temperature that prevents premature expansion. The intumescent material is prepared and mixed into the asphalt binder and polymer modifier at temperatures below the char-forming point, allowing it to be positioned in advance without triggering the expansion reaction. The actual expansion occurs later during fire exposure, not during manufacturing.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent applies parameter changes by controlling the temperature parameter during the incorporation of expandable graphite. The processing temperature is maintained below the char-forming temperature of the intumescent material during mixing and manufacturing steps. This temperature parameter control prevents premature expansion while still allowing the material to be incorporated. The temperature is then allowed to rise during fire exposure to trigger the desired expansion and flame resistance.

Inventive Principle:
Principle #35Parameter changes

2Ease of manufacture

If processing temperature is maintained below char-forming temperature to preserve intumescent material, then manufacturing feasibility is improved, but the scope of useful intumescent materials is restricted

Engineering Contradiction:
Improvemanufacturing feasibilityVSAvoidscope of useful materials
Core Design Contradiction:
Ease of manufactureVSAdaptability or versatility

Solution Approach 1:

The patent applies parameter changes by systematically controlling the temperature parameter to be below the char-forming temperature of the intumescent material during manufacturing. This temperature parameter control expands the scope of usable intumescent materials by preventing premature expansion reactions. The method allows various intumescent materials with different char-forming temperatures to be incorporated by simply adjusting the processing temperature to remain below their respective expansion points.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies preliminary action by incorporating the intumescent material into the asphaltic composition in advance at controlled temperatures. This preliminary incorporation at lower temperatures allows a broader range of intumescent materials to be used, as they are positioned in the composition before the final high-temperature steps. The material is prepared and mixed in advance without triggering expansion, expanding the versatility of usable materials.

Inventive Principle:
Principle #10Preliminary action

3Stability of the object's composition

If expandable graphite is added to hot asphaltic binder, then dispersion is improved, but premature expansion occurs which degrades the product

Engineering Contradiction:
Improvedispersion qualityVSAvoidpremature expansion
Core Design Contradiction:
Stability of the object's compositionVSObject-generated harmful factors

Solution Approach 1:

The patent applies parameter changes by controlling the temperature parameter to remain below the char-forming temperature of expandable graphite during the mixing and dispersion steps. This temperature control allows the graphite to be adequately dispersed in the asphaltic composition without triggering premature expansion. The temperature is maintained in a range that enables mixing while preventing the harmful expansion reaction.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies preliminary action by performing the dispersion and mixing of expandable graphite into the asphaltic binder at controlled lower temperatures before final processing. This preliminary mixing at lower temperatures achieves adequate dispersion of the graphite particles without causing premature expansion. The dispersion is established in advance under controlled conditions, preventing the harmful expansion effect.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method allows for the effective inclusion of expandable graphite in asphaltic sheets, enhancing fire resistance without deleterious expansion, thus expanding the scope of usable intumescent materials and improving manufacturing feasibility.

Implementation Method 1

expandable graphite...operating by forming a char layer...temperatures at which the asphaltic sheet can be manufactured or processed must be below the temperature at which the char layer forms

Methodology Applied
Scientific EffectThermal expansion: Thermal Expansion

Data Source

PatentUS10138375B2Method for manufacturing asphaltic sheet materials including expandable graphite
Publication Date: 2018.11.27 AMRIZE TECHNOLOGY SWITZERLAND LLC
  • US10138375B2 patent drawing

AI summary

A method for producing an asphaltic sheet having expandable graphite dispersed in one or more asphaltic components thereof, the method comprising: (i) preparing a masterbatch by combining asphalt binder and polymeric modifier at a first temperature; (ii) cooling the masterbatch to a second temperature, where the second temperature is lower than the first temperature; (iii) adding, after said step of cooling, expandable graphite to the masterbatch to thereby form an asphaltic composition including expandable graphite; and (iv) fabricating a sheet with the asphaltic composition including expandable graphite.