Asymmetric Wall-Flow Filter Washcoat Distribution

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Solution Overview

Problem

Current catalytic filtration systems for vehicular exhaust gases face challenges in achieving efficient NOx and soot removal due to the competition between reactions and high energy consumption in multi-step coating processes, which result in increased backpressure and resource utilization.

Innovation Solution

A catalysed wall-flow filter design with asymmetric honeycomb substrates, where the catalytic washcoat is applied differently to channels based on hydraulic diameter, allowing for selective coating on either channel walls or within the channels, and using a low-temperature setting cement for end-plugging to reduce process steps and energy requirements.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If multi-step coating processes are used to apply catalytic washcoat, then catalytic activity is improved, but process complexity and energy consumption increase

Engineering Contradiction:
Improvecatalytic activityVSAvoidprocess complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent combines multiple coating steps into a single washcoat application step. By formulating the washcoat slurry to contain catalyst precursors that are deposited simultaneously with the washcoat material, the process integrates what would traditionally require separate coating and catalyst impregnation steps, thereby reducing process complexity while maintaining catalytic activity

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The washcoat slurry serves multiple functions simultaneously: it provides the structural washcoat layer, delivers catalyst precursors to the substrate, and creates the catalytic active sites. This multi-functional approach eliminates the need for separate coating and catalyst application processes, reducing both process complexity and energy consumption

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Reliability

If multi-step coating processes are used to apply catalytic washcoat, then catalytic activity is improved, but energy consumption increases

Engineering Contradiction:
Improvecatalytic activityVSAvoidenergy consumption
Core Design Contradiction:
ReliabilityVSUse of energy by stationary object

Solution Approach 1:

The patent combines multiple coating steps into a single washcoat application step. By formulating the washcoat slurry to contain catalyst precursors that are deposited simultaneously with the washcoat material, the process integrates what would traditionally require separate coating and catalyst impregnation steps, thereby reducing process complexity while maintaining catalytic activity

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The catalyst precursors are pre-incorporated into the washcoat slurry before application. This preliminary incorporation ensures that the catalyst material is already positioned on the substrate when the washcoat is applied, eliminating the need for subsequent high-temperature calcination or catalyst activation steps that would consume additional energy

Inventive Principle:
Principle #10Preliminary action

3Manufacturing precision

If asymmetric honeycomb substrates with different channel hydraulic diameters are used, then washcoat distribution is optimized, but manufacturing complexity increases

Engineering Contradiction:
Improvewashcoat distributionVSAvoidsubstrate complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent employs an asymmetric honeycomb substrate design where inlet channels and outlet channels have different hydraulic diameters. This asymmetry creates differential capillary pressures during washcoat application, causing the washcoat slurry to be preferentially drawn into channels with larger hydraulic diameters. The result is optimized washcoat distribution that concentrates catalytic material where it is most needed, while the asymmetric geometry itself is a straightforward structural feature that does not significantly complicate manufacturing

Inventive Principle:
Principle #4Asymmetry

4Reliability

If washcoat is applied to all channels, then catalytic activity is maximized, but backpressure increases

Engineering Contradiction:
Improvecatalytic activityVSAvoidbackpressure
Core Design Contradiction:
ReliabilityVSStress or pressure

Solution Approach 1:

The patent applies washcoat preferentially to outlet channels rather than uniformly to all channels. The asymmetric honeycomb substrate design with larger outlet channel hydraulic diameters creates capillary forces that draw the washcoat slurry primarily into outlet channels during the coating process. This local concentration of catalytic material maximizes catalytic activity in the regions where it is most needed for exhaust gas treatment, while leaving inlet channels with minimal or no washcoat coating, thereby reducing overall backpressure across the filter

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design enhances NOx and soot removal efficiency while reducing backpressure and resource utilization by optimizing washcoat distribution and simplifying the coating process, allowing for improved performance with less energy and equipment usage.

Implementation Method 1

the liquid catalytic washcoat remains on a surface of the porous channel walls of the first channels or both remains on the surface of the porous channel walls and permeates the porous channel walls of the first channels

Methodology Applied
Scientific EffectCapillary action: Capillary Action

Implementation Method 2

a catalytic selective catalytic reduction (SCR) catalyst coating is disposed within a porous channel wall of the wall-flow filter and only on the outlet-wall because this design maximises both NO x removal and NO 2 -soot removal

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP3077083B1Wall-flow filter comprising catalytic washcoat
Publication Date: 2019.07.17 JOHNSON MATTHEY PLC
  • EP3077083B1 patent drawingFigure 1A~2B
  • EP3077083B1 patent drawingFigure 3~4
  • EP3077083B1 patent drawingFigure 5~6

AI summary

A catalysed honeycomb wall-flow filter for treating exhaust gas comprising particulate matter emitted from an internal combustion engine, which filter comprising a honeycomb substrate having a first end and a second end and comprising an array of interconnecting porous walls defining an array of longitudinally extending first channels and second channels, wherein the first channels are bordered on their sides by the second channels and have a larger hydraulic diameter than the second channels, wherein the first channels are end-plugged at a first end of the honeycomb substrate and the second channels are end-plugged at a second end of the honeycomb substrate, wherein channel wall surfaces of the first channels comprise an on-wall-type catalytic washcoat. The invention also relates to an exhaust system comprising the catalysed filter and to methods of making it.