Atomized Powder Ultrafine Particle Removal via Liquid Agitation

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Solution Overview

Problem

Reactive metal powders produced through atomization often contain ultrafine particles that adhere to fine particles, reducing flowability due to increased roughness and electromagnetic interactions, which existing sieving processes cannot effectively remove.

Innovation Solution

An ultrafine particle removal process involving the use of a removal liquid and energy addition, such as ultrasonic energy or mechanical agitation, to detach ultrafine particles from fine particles, followed by separation and recirculation of the removal liquid, enhancing the flowability of the resulting powder.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional sieving processes are used to separate particles, then particle size classification is achieved, but ultrafine particles adhering to fine particles cannot be effectively removed

Engineering Contradiction:
Improveparticle size classificationVSAvoidultrafine particle adhesion
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

A liquid medium is introduced as an intermediary between the ultrafine and fine particles. The liquid penetrates the interface between adhered particles, utilizing surface tension and wetting effects to separate the ultrafine particles from the fine particles, enabling effective removal that conventional dry sieving cannot achieve

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

Hydraulic action is employed by circulating liquid through the powder bed. The liquid flow generates shear forces and pressure differentials that detach ultrafine particles from fine particles, followed by filtration and recirculation of the liquid to continuously remove separated ultrafine particles

Inventive Principle:
Principle #29Pneumatics and hydraulics

2Productivity

If ultrafine particles are present on fine particles, then powder production is maintained, but flowability is reduced due to increased roughness and electromagnetic interactions

Engineering Contradiction:
Improvepowder productionVSAvoidflowability
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The harmful ultrafine particles are extracted and removed from the surface of fine particles using liquid penetration and hydraulic separation. This extraction process eliminates the sources of increased roughness and electromagnetic interactions, thereby restoring and improving powder flowability while maintaining production of usable fine powder

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The physical state and surface properties of particles are changed by introducing liquid medium. The liquid temporarily alters surface energy and inter-particle forces during processing, enabling separation. After liquid removal, particles exhibit improved flow characteristics due to reduced adhesion and roughness

Inventive Principle:
Principle #35Parameter changes

3Ease of operation

If removal liquid is used to detach ultrafine particles, then flowability is improved, but additional processing steps and equipment complexity are introduced

Engineering Contradiction:
ImproveflowabilityVSAvoidprocessing equipment
Core Design Contradiction:
Ease of operationVSDevice complexity

Solution Approach 1:

The removal liquid is filtered to separate and discard ultrafine particles, then the cleaned liquid is recirculated back into the system for continued use. This recovery and recirculation approach minimizes liquid consumption and reduces waste handling requirements, offsetting the added equipment complexity with operational efficiency

Inventive Principle:
Principle #34Discarding and recovering

Solution Approach 2:

The liquid medium serves multiple functions simultaneously: it acts as a separation agent to detach particles, as a transport medium to carry separated particles away, and as a recirculable resource that can be reused. This multi-functionality consolidates several process steps into one integrated system, reducing overall complexity

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Significantly improves the flowability of reactive metal powders by removing ultrafine particles, achieving a substantial increase in volumetric flowability and maintaining a high mass retention of the finished powder, suitable for applications like additive manufacturing.

Implementation Method 1

adding energy to a mixture of the atomized powder and the removal liquid to detach the ultrafine particles from the fine particles

Methodology Applied
Scientific EffectUltrasonic vibration: Ultrasonic Vibration

Implementation Method 2

adding energy to a mixture of the atomized powder and the removal liquid to detach the ultrafine particles from the fine particles

Methodology Applied
Scientific EffectMechanical agitation: Stirring

Implementation Method 3

contacting the atomized powder with a removal liquid to form a mixture of the atomized powder and the removal liquid

Methodology Applied
Scientific EffectWetting: Wetting

Implementation Method 4

separating the removal liquid and the ultrafine particles from the fine particles

Methodology Applied
Scientific EffectDensity gradient separation: Density Gradient

Implementation Method 5

adding energy to a mixture of the atomized powder and the removal liquid to detach the ultrafine particles from the fine particles

Methodology Applied
Scientific EffectKinetic energy input: Vibration

Data Source

PatentEP4491300A1System and method for atomized powder processing and a processed powder
Publication Date: 2025.01.15 GENERAL ELECTRIC CO
  • EP4491300A1 patent drawingFigure 1
  • EP4491300A1 patent drawingFigure 2
  • EP4491300A1 patent drawingFigure 3

AI summary

A method for removing ultrafine particles (206) from an atomized powder (306) is provided. The method includes contacting the atomized powder (306) with a removal liquid (324), the atomized powder (306) comprising fine particles (202) and ultrafine particles (206), wherein contacting the atomized powder (306) with the removal liquid (324) comprises adding energy to a mixture (336) of the atomized powder (306) and the removal liquid (324) to detach the ultrafine particles (206) from the fine particles (202); and separating the removal liquid (324) and ultrafine particles (206) from the fine particles (202).