Automated Calcimeter System for Carbonate Measurement

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Solution Overview

Problem

Current methods for measuring and analyzing carbonates in oil well cores or drill cuttings are prone to operator error due to the need for manual intervention, leading to potential misapplication of chemical treatments and increased downtime and costs.

Innovation Solution

An automated calcimeter system comprising a reservoir, pump, and reaction chamber that measures pressure changes caused by acid-carbonate reactions, allowing for automated data collection and comparison to calibration curves, reducing reliance on operator skill and minimizing errors.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If manual operator intervention is used to measure and analyze carbonates, then the process can be performed with simple equipment, but operator error increases and measurement accuracy decreases

Engineering Contradiction:
Improvecarbonate measurement accuracyVSAvoidsystem complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The system performs self-measurement and self-analysis of carbonate content through automated acid injection, pressure monitoring, and data processing. The microprocessor automatically compares measured pressure changes against stored calibration curves to determine carbonate content, eliminating the need for manual operator intervention and reducing human error while maintaining measurement accuracy.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The patent replaces manual mechanical operations (operators manually adding acid, reading pressure gauges, recording data) with an automated electronic system that uses a microprocessor to control acid injection timing, monitor pressure changes via sensor, and automatically analyze results by comparing data against stored calibration curves.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Reliability

If automated systems are implemented to eliminate operator error, then measurement accuracy improves, but device complexity increases

Engineering Contradiction:
Improveprocess reliabilityVSAvoidsystem complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The system achieves high reliability through self-service automation where the microprocessor controls the entire measurement process automatically - injecting acid at precise intervals, monitoring pressure changes, and analyzing results by comparing against stored calibration curves. This eliminates operator error and ensures consistent, reliable measurements without requiring complex manual procedures.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The system incorporates feedback mechanisms where the microprocessor continuously monitors pressure changes during the acid-carbonate reaction and automatically compares the measured data against stored calibration curves. This closed-loop feedback system ensures accurate determination of carbonate content and improves process reliability by automatically detecting and correcting measurement variations.

Inventive Principle:
Principle #23Feedback

3Productivity

If manual timing and data recording are used, then the equipment remains simple, but productivity decreases due to operator attention requirements

Engineering Contradiction:
Improvemeasurement throughputVSAvoidautomation complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The system enables continuous measurement operations by automatically injecting acid at predetermined intervals, continuously monitoring pressure changes, and immediately processing results. The microprocessor controls the timing and sequence of operations without interruption, allowing multiple samples to be analyzed in succession without requiring operator attention for timing or data recording, thus significantly improving measurement throughput.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The automated system performs all measurement and data processing functions without operator intervention - the microprocessor controls acid injection timing, monitors pressure changes automatically, and immediately analyzes results by comparing against stored calibration curves. This self-service capability eliminates bottlenecks caused by manual operations and increases productivity.

Inventive Principle:
Principle #25Self-service

4Loss of time

If operator skill and attentiveness are relied upon, then equipment complexity remains low, but loss of time increases due to potential errors requiring re-treatment

Engineering Contradiction:
Improvewell downtimeVSAvoidautomation complexity
Core Design Contradiction:
Loss of timeVSDevice complexity

Solution Approach 1:

The system eliminates time loss associated with operator errors by performing self-measurement and self-analysis with high accuracy. The microprocessor automatically determines carbonate content by comparing pressure data against stored calibration curves, ensuring correct chemical treatment selection on the first attempt and avoiding costly re-treatments that would extend well downtime.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The system uses feedback from pressure sensor data to automatically determine carbonate content and guide chemical treatment selection. By continuously monitoring the acid-carbonate reaction and comparing results against calibration curves, the system provides immediate, accurate feedback that prevents erroneous treatment decisions and reduces the need for repeated interventions, thereby minimizing well downtime.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The automated system enhances accuracy and efficiency by eliminating operator-dependent errors, reducing downtime and costs associated with ineffective treatments, and enabling precise chemical treatment applications.

Implementation Method 1

The amount of carbon dioxide gas produced may be measured using a pressure sensor

Methodology Applied
Scientific EffectPressure measurement:

Implementation Method 2

induce an acid-carbonate reaction where carbon dioxide may be released as a gas

Methodology Applied
Scientific EffectAcid-carbonate reaction: Chemical Bonding

Data Source

PatentUS9939361B2Automated calcimeter systems
Publication Date: 2018.04.10 HALLIBURTON ENERGY SERVICES INC
  • US9939361B2 patent drawing
  • US9939361B2 patent drawing
  • US9939361B2 patent drawing

AI summary

Automated calcimeter systems and methods of using the same are described. An automated calcimeter system may comprise a reaction chamber; a pressure sensor coupled to the reaction chamber and configured to measure pressure in the reaction chamber; a pump coupled to the reaction chamber; piping coupled to the pump, wherein the piping is of sufficient length to store a preselected volume of acid; and a processor configured to instruct the pump to deliver the preselected volume of acid to the reaction chamber while also drawing a volume of gas from the reaction chamber, wherein the volume of gas is equivalent to the preselected volume of acid.