Autosampler Gas Circulation for Uniform Sample Temperature

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Solution Overview

Problem

Existing autosamplers face challenges in uniformly adjusting the temperature of a sample plate, leading to temperature variations among samples, and require inefficient air temperature adjustments to achieve uniformity quickly.

Innovation Solution

An autosampler design featuring a sample storage space, a temperature adjustment space separated by a thermal insulation board with specific aperture ratios and distances, and a circulation device that adjusts gas temperature using radiators, ensuring uniform gas flow rates and efficient temperature adjustment.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If direct cooling method is used to adjust sample temperature quickly, then temperature adjustment speed is improved, but temperature distribution uniformity deteriorates

Engineering Contradiction:
Improvetemperature adjustment speedVSAvoidtemperature distribution uniformity
Core Design Contradiction:
SpeedVSTemperature

Solution Approach 1:

The cooling system is segmented into multiple independent cooling units, each equipped with its own heat exchanger and temperature control mechanism. This allows different regions of the sample plate to be cooled independently and simultaneously, achieving both fast temperature adjustment and uniform temperature distribution across all samples.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Each cooling unit is designed with locally optimized aperture ratios and heat exchanger configurations tailored to the specific thermal requirements of its region. The aperture ratios of communicating holes are adjusted according to position to ensure uniform gas flow rates and temperature distribution across different areas of the sample plate.

Inventive Principle:
Principle #3Local quality

2Temperature

If air temperature adjustment method is used to achieve uniform temperature distribution, then temperature uniformity is improved, but temperature adjustment efficiency deteriorates

Engineering Contradiction:
Improvetemperature distribution uniformityVSAvoidtemperature adjustment efficiency
Core Design Contradiction:
TemperatureVSProductivity

Solution Approach 1:

The air temperature adjustment system is divided into multiple independent cooling units, each capable of simultaneously adjusting the temperature of its designated region. This segmentation enables parallel temperature adjustment across the entire sample plate, maintaining uniformity while significantly improving adjustment speed and efficiency.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system uses gas circulation through communicating holes with optimized aperture ratios to transfer thermal energy efficiently. By controlling gas flow rates through pneumatic design, the system achieves rapid and uniform temperature adjustment across all samples without requiring direct contact cooling.

Inventive Principle:
Principle #29Pneumatics and hydraulics

3Ease of manufacture

If uniform aperture ratios are used in all cooling units, then manufacturing simplicity is improved, but gas flow uniformity deteriorates

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidgas flow uniformity
Core Design Contradiction:
Ease of manufactureVSTemperature

Solution Approach 1:

Each cooling unit is designed with locally optimized aperture ratios that vary according to its position and thermal requirements. This local customization ensures uniform gas flow rates and temperature distribution across all regions, with the trade-off managed through standardized modular designs that maintain reasonable manufacturing simplicity.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The aperture ratios of communicating holes are adjusted as a key parameter to optimize gas flow distribution. By changing the aperture ratios according to position and thermal requirements, the system achieves uniform temperature adjustment while maintaining manufacturing feasibility through systematic parameter optimization.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration allows for highly efficient temperature adjustment in the sample storage space, reducing temperature variations and improving the speed of achieving uniform sample temperatures.

Implementation Method 1

a heat exchanger that adjusts a temperature of gas flowing in the temperature adjustment space

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 2

a circulation device that causes gas to circulate between the sample storage space and the temperature adjustment space

Methodology Applied
Scientific EffectGas circulation: Convection

Data Source

PatentUS11953473B2Autosampler
Publication Date: 2024.04.09 SHIMADZU CORP
  • US11953473B2 patent drawing
  • US11953473B2 patent drawing
  • US11953473B2 patent drawing

AI summary

A circulation device causes gas to circulate between a sample storage space and a temperature adjustment space through the first and second opening regions in a separating member. A temperature of gas flowing in the temperature adjustment space is adjusted by a heat exchanger, so that the temperature of gas surrounding a sample in the sample storage space is adjusted. The separating member further has first and second unit regions. The second opening region includes a first portion located in the first unit region and a second portion located in the second unit region. The shortest distance between the first portion and the first opening region is larger than the shortest distance between the second portion and the first opening region, and an aperture ratio of the first portion in the first unit region is larger than an aperture ratio of the second portion in the second unit region.