Azoxystrobin Propiconazole Microemulsion Stability

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Solution Overview

Problem

Microemulsions of azoxystrobin, a fungicide with limited water solubility, tend to crystallize and lose stability over time, leading to reduced efficacy and storage issues in formulations without propiconazole.

Innovation Solution

A microemulsifiable concentrate comprising azoxystrobin, propiconazole, and an emulsifier system, which forms a stable oil-in-water microemulsion upon dilution with water, enhancing physical stability and biological efficacy.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If microemulsions of azoxystrobin are prepared without propiconazole, then the formulation is simpler, but the physical stability deteriorates due to crystallization over time

Engineering Contradiction:
Improveformulation complexityVSAvoidphysical stability
Core Design Contradiction:
Device complexityVSStability of the object's composition

Solution Approach 1:

The patent combines azoxystrobin with propiconazole in a microemulsifiable concentrate formulation. This merging of two different active ingredients resolves the technical contradiction by using propiconazole to prevent crystallization of azoxystrobin, thereby improving physical stability while maintaining reasonable formulation complexity through synergistic interaction between the two compounds

Inventive Principle:
Principle #5Merging (Combining)

2Quantity of substance

If azoxystrobin is used alone in microemulsion form, then the formulation has fewer components, but biological efficacy is reduced due to loss of stability

Engineering Contradiction:
Improvenumber of componentsVSAvoidbiological efficacy
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent merges azoxystrobin with propiconazole in a microemulsion formulation where propiconazole acts as a stabilizer that prevents crystallization of azoxystrobin. This combination maintains higher biological efficacy over time compared to azoxystrobin alone, as the stabilized formulation preserves the active ingredient's effectiveness throughout its shelf life and during application

Inventive Principle:
Principle #5Merging (Combining)

3Quantity of substance

If aromatic organic solvents are used to solubilize azoxystrobin, then solubility is improved, but ecological properties and toxicity worsen

Engineering Contradiction:
Improvewater solubilityVSAvoidecological toxicity
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The patent changes the formulation parameters by using a microemulsifiable concentrate system with propiconazole and surfactants instead of aromatic organic solvents. This parameter change achieves adequate solubility and dispersibility of azoxystrobin while significantly improving ecological properties and reducing toxicity, as microemulsions use water as the continuous phase and avoid harmful aromatic solvents

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The formulation exhibits prolonged physical stability and improved biological efficacy when diluted, maintaining stability and effectiveness in controlling fungal diseases.

Implementation Method 1

A microemulsifiable concentrate comprising azoxystrobin, propiconazole, and an emulsifier system, which forms a stable oil-in-water microemulsion upon dilution with water

Methodology Applied
Scientific EffectMicroemulsion: Microemulsion

Implementation Method 2

Microemulsions are a subclass of emulsions and are typically clear solutions. In general, microemulsions are characterised by emulsion droplets having average particle sizes between 0.01 and 0.1 micron

Methodology Applied
Scientific EffectEmulsion: Emulsion

Implementation Method 3

Microemulsions of azoxystrobin, a fungicide with limited water solubility, tend to crystallize and lose stability over time, leading to reduced efficacy and storage issues in formulations without propiconazole

Methodology Applied
Scientific EffectCrystallisation: Crystallisation

Data Source

PatentEP2004194B1Azoxystrobin formulations
Publication Date: 2016.04.27 SYNGENTA PARTICIPATIONS AG

AI summary

The present invention provides microemulsifiable concentrates and microemulsions comprising azoxystrobin and propiconazole.