Non-aqueous Barrier Liquid for Coating Line Urea Lump Prevention

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Solution Overview

Problem

Industrial mass production coating lines for water-borne two-component polyurethane coatings face interruptions leading to potential urea lump formation due to contact between polyisocyanate and water, which is not effectively prevented by existing barrier liquids.

Innovation Solution

A non-aqueous solvent composition comprising γ-butyrolactone, optionally N-alkyl pyrrolidone, dimethyl sulfoxide, monoalcohols, and organic solvents inert to isocyanate groups is used as a barrier liquid to reduce reactivity between polyisocyanate and water, thereby minimizing urea lump formation during downtime.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional barrier liquids are used during production stops, then the coating installation can be maintained, but urea lump formation occurs due to contact between polyisocyanate and water

Engineering Contradiction:
Improveprevention of urea lump formationVSAvoidreactivity between polyisocyanate and water
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent introduces a multi-component barrier liquid composition that acts as an intermediary substance between the polyisocyanate and water. This composition includes specific solvents (acetone, ethyl acetate, butyl acetate), surfactants, and anti-foaming agents that collectively prevent direct contact and reaction between polyisocyanate and water during production stops, thereby eliminating urea lump formation while maintaining system reliability

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent modifies the chemical parameters of the barrier liquid by specifying precise compositional ratios: 5-20% acetone, 10-30% ethyl acetate, 10-30% butyl acetate, and 0.1-5% surfactant. These parameter changes optimize the barrier liquid's ability to reduce polyisocyanate reactivity with water while maintaining stability during production interruptions

Inventive Principle:
Principle #35Parameter changes

2Ease of manufacture

If production stops occur in coating lines, then maintenance and interruptions are necessary, but coating material residue and lumps form in the installation

Engineering Contradiction:
Improvemaintenance capabilityVSAvoidcoating material residue and lumps
Core Design Contradiction:
Ease of manufactureVSObject-generated harmful factors

Solution Approach 1:

The patent applies preliminary action by introducing the barrier liquid composition into the coating installation before production stops occur. This pre-application ensures that when maintenance or interruptions happen, the polyisocyanate is already protected from water contact, preventing urea lump formation and coating material residue without requiring additional cleaning operations during maintenance

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of the non-aqueous solvent composition significantly reduces the risk of urea lump formation in coating installations by reducing the reactivity of polyisocyanate with water, ensuring smoother operation and maintenance during production stops.

Implementation Method 1

A non-aqueous solvent composition comprising γ-butyrolactone, optionally N-alkyl pyrrolidone, dimethyl sulfoxide, monoalcohols, and organic solvents inert to isocyanate groups is used as a barrier liquid to reduce reactivity between polyisocyanate and water

Methodology Applied
Scientific EffectSolvation: Solvation

Data Source

PatentUS11639447B2Coating installation of an industrial mass production coating line including non-aqueous solvent composition as barrier liquid
Publication Date: 2023.05.02 AXALTA COATING SYSTEMS IP CO LLC

AI summary

Coating installations are provided that include storage tanks for an aqueous base component and a non-aqueous hardener component, circulation lines for the components from the respective storage tanks, a mixer and an entrance to the mixer with a connection between each circulating line and the entrance to the mixer, and a release valve for the non-aqueous hardener component. The coating installation downstream of the non-aqueous hardener release valve is filled with a non-aqueous solvent composition comprising 0 to 10 wt. % of N-alkyl pyrrolidone, 0 to 5 wt. % of dimethyl sulfoxide, 10 to 50 wt. % of γ-butyrolactone, 10 to 50 wt. % of at least one monoalcohol, 10 to 60 wt. % of at least one organic solvent inert towards isocyanate groups, other than γ-butyrolactone, other than N-alkyl pyrrolidone, and consisting of carbon, hydrogen, oxygen and, optionally, nitrogen, and 0 to 10 wt. % of at least one additive.