Batch Chemical Reactor Segmentation for Research-to-Production Transition

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Solution Overview

Problem

Prior art chemical reactors face issues with lengthy transition times and high costs from the research phase to production, high energy consumption, and rigidity in production systems due to lack of standardized yield and real-time energy monitoring and control.

Innovation Solution

A batch-type chemical reactor with a main body, hermetically sealed head element, and discretizing elements that allow for three-dimensional manipulation of reaction kinetics and energy, enabling real-time monitoring and control of process parameters, and standardization of chemical mixtures irrespective of reaction volumes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If prior art reactors are designed for specific production volumes, then they can handle designated reaction scales, but they result in high rigidity of production systems and lengthy transition times between research and production phases

Engineering Contradiction:
Improveadaptability to different reaction volumesVSAvoidtransition time from research to production phase
Core Design Contradiction:
Adaptability or versatilityVSLoss of time

Solution Approach 1:

The reactor is divided into multiple discrete reaction chambers (first reaction chamber, second reaction chamber, third reaction chamber) that can be independently controlled and operated. This segmentation allows the system to handle different reaction volumes and types simultaneously, enabling seamless transition from research-scale to production-scale operations without requiring system replacement.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The reactor system is designed with multi-functional capabilities to perform diverse chemical reactions (oxidation, reduction, hydrolysis, condensation, polymerization) within the same apparatus. The universal design includes standardized interfaces, common control systems, and interchangeable reaction chambers, allowing the same reactor to serve both research and production phases without transition delays.

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Use of energy by moving object

If prior art reactors operate without real-time energy monitoring, then they have simpler control systems, but they result in high energy consumption and inability to manipulate internal reaction energy

Engineering Contradiction:
Improveenergy consumptionVSAvoidcomplexity of energy monitoring and control system
Core Design Contradiction:
Use of energy by moving objectVSDevice complexity

Solution Approach 1:

The reactor incorporates temperature sensors, pressure sensors, and flow meters that continuously monitor reaction conditions and provide real-time feedback to the control system. This feedback mechanism enables dynamic adjustment of heating, cooling, and reagent addition rates to optimize energy consumption while maintaining precise control over reaction energy and conditions.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The system replaces manual energy management with automated electronic control systems that use sensors and actuators to manipulate reaction energy. The control system electronically regulates heating elements, cooling systems, and reagent flow rates, substituting mechanical intuition with precise electronic measurement and control to reduce energy waste.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Manufacturing precision

If prior art reactors lack real-time monitoring capabilities, then they have simpler structures, but they result in inability to achieve maximum uniformity of process conditions and standardized yield

Engineering Contradiction:
Improveuniformity of process conditionsVSAvoidcomplexity of monitoring and control devices
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

Multiple sensors (temperature, pressure, flow) are distributed throughout the reactor system to continuously monitor process conditions in real-time. This feedback is processed by the control system which automatically adjusts operational parameters to maintain uniform conditions across all reaction chambers, ensuring consistent yield and product quality regardless of reaction volume or type.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The reactor system employs dynamic control mechanisms that continuously adapt operational parameters based on real-time sensor data. Heating rates, cooling rates, reagent flow rates, and agitation speeds are dynamically adjusted to compensate for variations in reaction progress, ensuring maximum uniformity of process conditions throughout the reaction and enabling standardized yield across different production scales.

Inventive Principle:
Principle #15Dynamics

4Ease of manufacture

If prior art reactors use non-standardized processes for different volumes, then they have greater flexibility in handling various reaction types, but they result in high costs during passage from research to production phase

Engineering Contradiction:
Improvecost of process transitionVSAvoidability to handle different reaction volumes
Core Design Contradiction:
Ease of manufactureVSAdaptability or versatility

Solution Approach 1:

The reactor system uses modular, interchangeable reaction chambers that can be easily swapped or reconfigured based on production needs. This segmentation allows the same base system to handle both small-scale research reactions and large-scale production reactions, eliminating the need for separate equipment investments and reducing transition costs between phases.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The reactor is designed as a universal platform capable of performing multiple reaction types (oxidation, reduction, hydrolysis, condensation, polymerization) and handling various volumes within the same system. This multi-functionality is achieved through standardized interfaces, common utility connections, and programmable control systems, thereby eliminating the need for separate specialized equipment for research and production, significantly reducing transition costs.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Data Source

PatentUS20230149886A1Chemical reactor
Publication Date: 2023.05.18 B4CHEM SRL
  • US20230149886A1 patent drawing
  • US20230149886A1 patent drawing
  • US20230149886A1 patent drawing

AI summary

Described is a chemical reactor, in particular of the batch type, including a main body defining a reaction space for chemical processes, a head element configured to hermetically seal the main body, a supporting base designed to contain the main body and a plurality of discretizing elements, which are anchored or can be anchored to the head element and extending inside said main body according to a main direction of extension, configured to discretize the process operations into sub-spaces for releasing activation energy.The head element is movable in such a way as to form, using said discretizing elements, controlled mixing of the reactions and measurements, preferably density measurements, of the solutions.