Solid-State Battery Slurry Mixing for Fluidity and Ion Conductivity

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Solution Overview

Problem

Conventional slurry compositions for all-solid-state secondary batteries face challenges in enhancing fluidity, preservation stability, and ion conductivity of the solid electrolyte-containing layers.

Innovation Solution

A slurry composition comprising a solid electrolyte, a polymer, and a solvent, with a specific fineness of grind ratio relative to the average primary particle diameter of the solid electrolyte, and incorporating vinyl cyanide and (meth)acrylic acid ester monomer units, which improves fluidity and ion conductivity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If conventional slurry composition is used, then basic battery structure is formed, but fluidity and preservation stability are insufficient

Engineering Contradiction:
ImprovefluidityVSAvoidpreservation stability
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent applies parameter changes by carefully controlling the fineness of grind of the solid electrolyte and the average primary particle diameter within specific ranges. This optimization of physical parameters enables the slurry to achieve both excellent fluidity for easy application and preservation stability for reliable storage, resolving the technical contradiction between ease of operation and reliability.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If conventional slurry composition is used, then electrode layer is formed, but ion conductivity is insufficient

Engineering Contradiction:
Improveion conductivityVSAvoidslurry composition complexity
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent achieves high ion conductivity by optimizing physical parameters including the fineness of grind of solid electrolyte (0.1-10 μm) and average primary particle diameter (1-100 nm), rather than complicating the slurry composition. This parameter optimization approach improves reliability while maintaining ease of manufacture.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If solid electrolyte particle size is reduced, then ion conductivity improves, but fluidity and preservation stability deteriorate

Engineering Contradiction:
Improveion conductivityVSAvoidfluidity
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The patent resolves this contradiction by precisely controlling two parameters: the fineness of grind (0.1-10 μm) and average primary particle diameter (1-100 nm) within specific ranges. This dual parameter optimization ensures that the solid electrolyte maintains high ion conductivity while the slurry retains excellent fluidity and preservation stability.

Inventive Principle:
Principle #35Parameter changes

4Reliability

If solid electrolyte particle size is reduced, then ion conductivity improves, but preservation stability deteriorates

Engineering Contradiction:
Improveion conductivityVSAvoidpreservation stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent simultaneously optimizes the fineness of grind (0.1-10 μm) and average primary particle diameter (1-100 nm) to achieve a balance where high ion conductivity is maintained while preservation stability is improved. The specific parameter ranges prevent excessive particle reduction that would harm stability.

Inventive Principle:
Principle #35Parameter changes

Data Source

PatentUS20240413381A1Method of producing slurry composition for all-solid-state secondary battery
Publication Date: 2024.12.12 ZEON CORP

AI summary

A method of producing a slurry composition for an all-solid-state secondary battery is provided. The method includes: a step of performing mixing treatment with respect to a composition that contains a solid electrolyte, a polymer, and a solvent and that has a solid content concentration of 70 mass % or more to produce a preliminary mixture; a step of further adding a solvent to the preliminary mixture having a solid content concentration of 70 mass % or more to obtain a diluted material having a solid content concentration of more than 40 mass % and less than 70 mass %; a step of performing kneading treatment with respect to the diluted material having a solid content concentration of more than 40 mass % and less than 70 mass % to produce a kneaded material; and a step of further adding a solvent to the kneaded material to dilute the kneaded material.